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e-<strong>conservation</strong><br />

<strong>the</strong> <strong>online</strong> magazine No. <strong>16</strong>, October 2010


Contemporary Art Wall Clock by PaulaArt


The Gap in Conservation<br />

In recent conversations with fresh PhD graduates I have unfortunately noticed an increasing tendency:<br />

towards unemployment. To a conservator-restorer or a <strong>conservation</strong>-scientist, a PhD is synonym of<br />

higher specialisation, also a better job and a higher salary. At least that is <strong>the</strong> illusion that exists<br />

before one obtains it.<br />

For some, a PhD is a life goal worthy of achievement. For o<strong>the</strong>rs, it is merely a means to reach an objective,<br />

usually to ensure a university position. Independently of <strong>the</strong> reason why one does it, it is true that <strong>the</strong>re is<br />

a life before <strong>the</strong> PhD and ano<strong>the</strong>r after it. More and more, life before <strong>the</strong> PhD is full of expectations<br />

while life after it is quite different than one would have imagined, often in a very disappointing way.<br />

This is not a problem restricted to <strong>conservation</strong>, but it's becoming more and more accentuated<br />

because PhDs in our field are a fairly recent thing, most being less than 10 years old. Despite that,<br />

PhD programs seem to create problems instead of filling <strong>the</strong> gaps in our training or solving <strong>the</strong><br />

problems in <strong>the</strong> field of cultural heritage.<br />

Part of <strong>the</strong> problem is in <strong>the</strong> academic sphere itself: after all <strong>the</strong>re is definitely a market for training<br />

PhD students. It's academic economics and it’s all about demand and supply. When a university<br />

creates a PhD program it attracts more students, increases funds and raises status. After all, it is a<br />

business like any o<strong>the</strong>r and more than ever universities are competing with one ano<strong>the</strong>r. But <strong>the</strong><br />

bitter truth is that Academia doesn't really care about <strong>the</strong>ir students' career prospects. The goal is to<br />

have lots of students in order to help support <strong>the</strong>ir facilities and <strong>the</strong>ir staff, staff which are required<br />

to have a PhD. Even if you do eventually get a university position, you must bring in a new generation<br />

of students to keep afloat <strong>the</strong> department and subsequently your own job, perpetuating <strong>the</strong> system<br />

and thus, <strong>the</strong> problem.<br />

In <strong>the</strong> last decade several PhD courses have appeared in European Universities, in some countries<br />

more than o<strong>the</strong>rs, in order to offer <strong>the</strong> three different levels of European tertiary education and to<br />

be one of <strong>the</strong> exclusive “few” to do so. When PhD students graduate some are absorbed by Academia<br />

to complement <strong>the</strong>ir staff, normally as post-d<strong>oct</strong>orates with scholarships, while o<strong>the</strong>rs are left “on<br />

<strong>the</strong>ir own”. At <strong>the</strong> end of <strong>the</strong> day, PhDs are low-paid and treated as merely temporary workers during<br />

<strong>the</strong> years <strong>the</strong>y spend training for faculty positions that are virtually inexistent.<br />

What is <strong>the</strong> result of <strong>the</strong> current scenario Unturn any stone and you will find many unemployed<br />

D<strong>oct</strong>orate graduates, o<strong>the</strong>rs surviving on public funding, or going from post-doc to post-doc<br />

anywhere <strong>the</strong>y can. Many resigning <strong>the</strong>mselves and settle for lower job positions, which in <strong>the</strong> present<br />

economical climate are also hard to find.<br />

Opposed to Academia, o<strong>the</strong>r fields have <strong>the</strong> Industry which absorbs a great part of PhD graduates.<br />

However, this is practically non-existent in <strong>conservation</strong> and clearly insufficient to absorb many of<br />

<strong>the</strong> hundreds of highly skilled D<strong>oct</strong>ors that are being trained every year.<br />

On <strong>the</strong> o<strong>the</strong>r side, politics are a great part of <strong>the</strong> problem. When government funding is common<br />

knowledge and widely available, students often consider pursuing a PhD because it ensures an<br />

income for at least a few years. But in fact this is all part of a bigger scheme that starts by attracting<br />

students to undergraduate <strong>conservation</strong>-restoration courses, often lured in by <strong>the</strong> highly publicized<br />

popular idea that if <strong>the</strong>re is cultural heritage in need of <strong>conservation</strong> it is because <strong>the</strong>re's a lack of<br />

professionals to conserve or restore it. Far from <strong>the</strong> truth, <strong>the</strong>se new generations, attracted by a real<br />

interest in heritage, will later join <strong>the</strong> increasingly large mass of skilful but unemployed professionals.<br />

This is equally true for <strong>conservation</strong>-scientists who often specialize in heritage during <strong>the</strong>ir PhD<br />

<strong>the</strong>sis. It may be a much needed area of input, but while <strong>the</strong> training programs are increasing I don't<br />

see a higher number of positions being filled or even on offer for that matter.<br />

When will this paradigm change Is it likely that this will only happen when <strong>the</strong> system is already<br />

near a state of absolute collapse Right now, it simply doesn't pay to get a PhD.<br />

editorial<br />

Rui Bordalo<br />

Editor-in-Chief<br />

e-<strong>conservation</strong>


PROFILE<br />

Location<br />

The Metropolitan Museum of Art<br />

Exhibition<br />

Picasso in The Metropolitan Museum of Art<br />

Time<br />

April 27, 2010 – August 15, 2010<br />

Glazing<br />

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solution for your demanding frame and display requirements.<br />

Optium combines <strong>the</strong> best of both worlds, anti-reflective safety glass and UV filtering acrylic, in<br />

one product, for all your design and <strong>conservation</strong> needs. Find out why museums around <strong>the</strong> world<br />

depend on Optium to protect, conserve and display <strong>the</strong>ir most valuable and historic collections.<br />

Optium. The Difference is Clear .<br />

To experience <strong>the</strong> clear difference, contact your authorized supplier for<br />

a free Optium Sample Kit or visit www.tru-vue.com/museums/econ.<br />

Pablo Picasso, At <strong>the</strong> Lapin Agile, 1905, The Walter H. and Leonore Annenberg Collection, Gift of<br />

Walter H. and Leonore Annenberg, 1992, Bequest of Walter H. Annenberg, 2002 (1992.391); The Actor,<br />

1904–05, Gift of Thelma Chrysler Foy, 1952 (52.175); Saltimbanque in Profile, 1905, Bequest of Scofield<br />

Thayer, 1982 (1984.433.269). All works from The Metropolitan Museum of Art. © 2010 Estate of Pablo<br />

Picasso / Artists Rights Society (ARS), New York. Photo: Don Pollard.<br />

Tru Vue ® , <strong>the</strong> Tru Vue logo, Optium ® , Optium Acrylic ® and Optium Museum Acrylic ® are registered<br />

trademarks, and Optium ® Museum Display Acrylic is a trademark of Tru Vue, Inc, McCook, IL USA.<br />

© 2010 Copyright Tru Vue, Inc. All rights reserved.<br />

Follow Us:


INDEX<br />

NEWS & VIEWS 6<br />

Pot Healer, I Need You<br />

By Daniel Cull<br />

9<br />

REVIEWS<br />

SEM and Microanalysis in <strong>the</strong> Study of Historical Technology,<br />

Materials and Conservation<br />

September 9-10, 2010, London, UK<br />

Review by Ana Bidarra<br />

13<br />

Western Association for Art Conservation (WAAC) Annual Meeting<br />

September 15 - 18, 2010, Portland, Oregon<br />

Review by Daniel Cull<br />

17<br />

NEWS<br />

Devastating Flood in Ladakh, India<br />

A Support Program by Tibet Heritage Fund<br />

By Andre Alexander<br />

EVENTS<br />

20<br />

UPCOMING EVENTS<br />

November 2010<br />

ARTICLES<br />

24<br />

Identification of Ivory Book Covers and Comparison to Ivory<br />

Portrait Miniatures<br />

By Josie Wornoff<br />

39<br />

Microbial Study of Egyptian Mummies<br />

An Assessment of Enzyme Activity, Fungicides and Some<br />

Mummification Materials for <strong>the</strong> Inhibition of Microbial Deterioration<br />

by Abdelrazek Elnaggar, Ahmed Sahab, Siham Ismail, Gamal Mahgoub and<br />

Mohammed Abdelhady<br />

CASE STUDY<br />

50<br />

Study of <strong>the</strong> painting Virgin Mary and Child with <strong>the</strong> Infant<br />

St. John <strong>the</strong> Baptist<br />

The Hidden Flora of Leonardo da Vinci’s Painting Workshop<br />

By Miklós Szentkirályi<br />

60<br />

"The Annunciation" by Cola Petruccioli (1380)<br />

The Restoration of <strong>the</strong> Transferred Wall Painting<br />

By Ildikó Jeszeniczky<br />

e-<strong>conservation</strong><br />

5


news & views<br />

POT HEALER, I NEED YOU<br />

By Daniel Cull<br />

"I like to build universes that do fall apart [...] objects, customs, habits, and ways of life<br />

must perish so that <strong>the</strong> au<strong>the</strong>ntic human being can live." (Philip K. Dick).[1]<br />

Conservators, and <strong>conservation</strong>, appear<br />

in numerous fictional books,<br />

films, and TV shows [2], I'd like to<br />

suggest that studying fiction is a<br />

fascinating, albeit underutilized,<br />

approach to a range of <strong>conservation</strong><br />

studies, not least because our portrayal<br />

within <strong>the</strong> fictional realm feeds<br />

directly into <strong>the</strong> public consciousness,<br />

and perception, of our profession. I<br />

recently read <strong>the</strong> Philip K. Dick (PKD)<br />

novel "Galactic Pot Healer" (GPH)<br />

[3], and was struck by how it can be<br />

read in contrast with contemporary<br />

museum based futurism, and as a<br />

work of <strong>conservation</strong> (pot-healing)<br />

<strong>the</strong>ory. Museum futurists predict that<br />

a continuing desire for '<strong>the</strong> real' will<br />

maintain a central significance in <strong>the</strong><br />

museum project for <strong>conservation</strong> [4].<br />

PKD, however, offers a different prediction.<br />

In GPH our protagonist, a<br />

healer of pots named Joe Fernwright, Book cover. Photo by Chris Drumm, Some rights reserved.<br />

inhabits a world in which ceramics<br />

have been replaced by plastic, and In what's called 'soft' science fiction it is <strong>the</strong> story<br />

where all <strong>the</strong> ceramics in museums that holds more value than scientific gizmo's.<br />

have been ‘healed’. PKD reveals <strong>the</strong> However, as scientists, it can be fun to consider<br />

utopic vision of classical <strong>conservation</strong><br />

<strong>the</strong>ory to be a dystopia in which our fictional selves have dreamt up; and consider<br />

what improvements to our field <strong>the</strong> writers of<br />

conservators are all but obsolete, whe<strong>the</strong>r <strong>the</strong>y could, as with <strong>the</strong> needle-less injection<br />

from Star Trek, become reality. GPH fea-<br />

and Joe passes his time playing<br />

"<strong>the</strong> game" and craving illegal cigarettes.<br />

vation scientists, including; self focusing<br />

tures several intriguing challenges for consermagni-<br />

e-<strong>conservation</strong>


VIEWS<br />

fying glasses, heat needles that bond <strong>the</strong> ceramic<br />

on <strong>the</strong> molecular level (I'm pretty sure that's<br />

non-reversible!), and replacing <strong>the</strong> ceramic conservators<br />

sand-box with an anti-gravity machine<br />

and storage boxes that if dropped gently slow<br />

<strong>the</strong>ir rate of descent before landing safely on<br />

<strong>the</strong> ground. Notwithstanding such leaps in technology,<br />

I suspect conservators can take more<br />

from <strong>the</strong> story than <strong>the</strong>se tools. Back in <strong>the</strong> Communal<br />

North American Citizen's Republic, Joe's<br />

routine existence is interrupted when he receives<br />

a message: "Pot healer, I need you. And I will pay"<br />

[3, p.12]. As his curiosity is awakened he discovers<br />

that on ano<strong>the</strong>r planet <strong>the</strong> Glimmung "intended<br />

to raise <strong>the</strong> ancient ca<strong>the</strong>dral Heldscalla, and to<br />

do so [...] needed a wide span of skills" [3, p. 25];<br />

amongst <strong>the</strong>m a pot-healer. As <strong>the</strong> plot develops<br />

Joe undergoes a variety of adventures and struggles,<br />

he gives all his savings away, has a run in<br />

with <strong>the</strong> Quietude Authority Police, travels to a<br />

different planet, falls in love, challenges <strong>the</strong> apparent<br />

precognition of <strong>the</strong> 'Book of <strong>the</strong> Kalends',<br />

and undergoes an epic struggle to raise <strong>the</strong> ca<strong>the</strong>dral,<br />

before finally coming to a decision regarding<br />

his future as a pot-healer. As a conservator it is<br />

possible to read Joe's personal and spiritually<br />

gnostic journey through <strong>the</strong> prism of investigative<br />

cleaning, <strong>the</strong> methodical uncovering of layers to<br />

reveal new realities below. As our reality becomes<br />

increasingly fluid and fleeting <strong>the</strong> book provides<br />

an intriguing metaphor for contemporary readings<br />

of au<strong>the</strong>nticity.<br />

The final section of <strong>the</strong> novel offers an interesting<br />

challenge to museum futurists, and <strong>conservation</strong><br />

<strong>the</strong>orists. PKD posits a post-enlightenment,<br />

experiential, reading of material culture, which<br />

contrasts with how <strong>the</strong> <strong>conservation</strong> object has<br />

traditionally been seen as "an object of <strong>the</strong> Enlightenment,<br />

an object that can be known through<br />

scientific analysis" [5]. In our world such distinctions<br />

are already becoming blurred with <strong>the</strong> advent<br />

of replicas, copies, fakes, forgeries, virtual<br />

collections, and simulations. Moreover, developments<br />

in ethnographic and contemporary art <strong>conservation</strong><br />

have led <strong>the</strong> <strong>conservation</strong> process to<br />

increasingly be concerned with meanings, and<br />

au<strong>the</strong>nticity, and not solely <strong>the</strong> materiality of<br />

objects. It has been suggested we "confront <strong>the</strong><br />

thingness of objects when <strong>the</strong>y stop working for<br />

us [...] when <strong>the</strong>ir flow within <strong>the</strong> circuits of production<br />

and distribution, consumption and exhibition,<br />

has been arrested, however momentarily"<br />

[6]. This being <strong>the</strong> case <strong>the</strong> focus of <strong>conservation</strong><br />

cannot solely be <strong>the</strong> object, but, also must be <strong>the</strong><br />

mechanism of its flow. By making his first pot Joe<br />

seeks to (re)create his traditional material culture,<br />

and satisfy his desire for cultural meaning.<br />

Perhaps too this illustrates <strong>the</strong> authors own approach<br />

to personal and cultural au<strong>the</strong>nticity, creating<br />

worlds in which things do fall apart; worlds<br />

in which maybe <strong>conservation</strong> does, after all, have<br />

a role to play:<br />

“He appraised what he had done, and, within it,<br />

what he would do, what later pots would be like,<br />

<strong>the</strong> future of <strong>the</strong>m lying before him. And his justification,<br />

in a sense, for leaving Glimmung and<br />

all <strong>the</strong> o<strong>the</strong>rs. Mali, <strong>the</strong> most of all. Mali whom<br />

he loved.<br />

The pot was awful.” [3, p. 144]<br />

Notes:<br />

1. Quoted in: Vincent Bzdek. Philip K. Dick's<br />

Future is Now. The Washington Post, Sunday<br />

July 28, 2002, URL.<br />

2. Rebecca A. Rushfield. Conservation Fiction<br />

(or Fiction that Acknowledges <strong>the</strong> Existence<br />

of Conservation and Conservators), URL, and<br />

Canadian Association for Conservation.<br />

Conservation in Film and Fiction, URL.<br />

e-<strong>conservation</strong> 7


VIEWS<br />

3. Philip K. Dick, Galactic Pot-healer, Berkley,<br />

1969.<br />

4. Center for <strong>the</strong> Future of Museums, Museums<br />

and Society 2034: Trends and Potential Futures.<br />

Version 1.0. Center for <strong>the</strong> Future of<br />

Museums/American Association of Museums.<br />

December 2008, URL [pdf].<br />

5. Pip Laurenson. Au<strong>the</strong>nticity, Change and Loss<br />

in <strong>the</strong> Conservation of Time-Based Media Installations.<br />

Tate Papers. Autumn 2006, URL.<br />

6. Bill Brown. Thing Theory. Critical Inquiry, Vol.<br />

28, No. 1. Things (Autumn, 2001). pp. 4.<br />

The News section is publishing diverse<br />

information on cultural heritage topics, such<br />

as on-site <strong>conservation</strong> projects reports,<br />

conferences, lectures, talks or workshops<br />

reviews, but also course reviews and any o<strong>the</strong>r<br />

kind of appropriate announcements. If you are<br />

involved in interesting projects and you want<br />

to share your experience with everybody else,<br />

please send us your news or announcements.<br />

For more details, such as deadlines and<br />

publication guidelines, please visit<br />

www.e-<strong>conservation</strong>line.com<br />

DANIEL CULL<br />

Conservator<br />

The Musical Instrument Museum<br />

Daniel Cull is from <strong>the</strong> West Country of <strong>the</strong> British<br />

Isles. He trained at <strong>the</strong> Institute of Archaeology,<br />

University College London, where he received a<br />

BSc in Archaeology, MA in Principles of <strong>conservation</strong>,<br />

and an MSc in Conservation for Archaeology<br />

and Museums. He was later awarded an Andrew<br />

W. Mellon Fellowship at <strong>the</strong> National Museum of<br />

<strong>the</strong> American Indian/Smithsonian Institution,<br />

Washington, DC. He currently works as a conservator<br />

at <strong>the</strong> Musical Instrument Museum and as<br />

a collaborator with e-<strong>conservation</strong> magazine.<br />

Website: http://dancull.wordpress.com<br />

Contact: daniel.cull@<strong>the</strong>mim.org<br />

8 e-<strong>conservation</strong>


REVIEWS<br />

SEM AND MICROANALYSIS IN THE STUDY OF<br />

HISTORICAL TECHNOLOGY, MATERIALS AND CONSERVATION<br />

Review by Ana Bidarra<br />

September 9-10, 2010<br />

London, UK<br />

Organisers:<br />

The British Museum and<br />

Hitachi High Technologies Europe<br />

http://www.britishmuseum.org/...<br />

On 9 th and 10 th September 2010, <strong>the</strong> Department<br />

of Conservation and Scientific Research at <strong>the</strong><br />

British Museum, in association with Hitachi High<br />

Technologies Europe, hosted a conference on <strong>the</strong><br />

application of scanning electron microscopy and<br />

microanalysis (SEM-EDX) to <strong>the</strong> study of materials,<br />

manufacturing methods and deterioration processes<br />

of objects from ancient to contemporary<br />

cultures. The conference was attended by over<br />

150 delegates representing 22 countries (including<br />

North, Central and South America, China,<br />

Japan, Iran and most European countries). There<br />

were 28 oral presentations and 45 posters divided<br />

in 2 sessions over <strong>the</strong> 2-days conference.<br />

The presentations focused on several areas of study,<br />

from broader applications of SEM and microanalysis<br />

techniques, to specific case studies, technological<br />

advances and limitations. The conference<br />

started with a presentation from Alexander Ball<br />

entitled How “non-destructive” is variable pressure<br />

SEM, introducing some basic concepts of<br />

variable pressure SEM focusing on <strong>the</strong> alterations<br />

caused by <strong>the</strong> technique due to <strong>the</strong> effects of rapid<br />

decompression, beam interactions between <strong>the</strong><br />

samples and imaging gas and <strong>the</strong> contamination<br />

from <strong>the</strong> vacuum system. These effects can cause<br />

cracking, contaminations, dehydration, radiation<br />

damages, etc. It was an alert call, particularly<br />

directed to <strong>the</strong> recent possibilities of analysing<br />

entire objects, since modern equipments have<br />

bigger vacuum chambers. The first session ended<br />

with two presentations on <strong>the</strong> study of parchment<br />

biodegradation and on <strong>the</strong> study of glass beads<br />

from urns found in 1970 in an excavation in Carthage,<br />

followed by <strong>the</strong> first poster session.<br />

The second session began with a practical approach<br />

on <strong>the</strong> use of SEM in <strong>the</strong> study of surface materials<br />

at high magnification. Ineke Joosten focused on<br />

<strong>the</strong> parameters that could influence <strong>the</strong> image such<br />

as scan rotation, magnification, beam voltage,<br />

type of detector and pressure in <strong>the</strong> vacuum chamber.<br />

In <strong>the</strong> second presentation, Caroline Cartwright<br />

introduced a very interesting application<br />

of SEM to <strong>the</strong> study of <strong>the</strong> organic cores from <strong>the</strong><br />

Iron Age Snettisham (Norfolk) torc hoard, from<br />

around 70 BC. The study added important new information<br />

regarding <strong>the</strong> manufacture of <strong>the</strong>se objects.<br />

The last session was on <strong>the</strong> study of <strong>the</strong> Bedford<br />

Lemere Collection, particularly <strong>the</strong> deterioration of<br />

glass plate negatives from mid to late 19 th century.<br />

e-<strong>conservation</strong> 9


REVIEWS<br />

The afternoon session focused on four different<br />

<strong>the</strong>mes: smalt pigment quantitative EDX analysis;<br />

medieval window flashed glass composition, structure<br />

and manufacturing processes; organic remains<br />

preserved by metal corrosion products;<br />

and a multi-analytical study of <strong>the</strong> pigments in<br />

17 th century Portuguese tiles (“azulejos”). The<br />

first presentation, by Marika Spring, introduced<br />

several examples of SEM-EDX analysis on smalt<br />

samples from a number of paintings in <strong>the</strong> National<br />

Gallery ranging in date and geographical<br />

origin. The variations in arsenic content as well<br />

as possible effects of arsenic on <strong>the</strong> properties<br />

of <strong>the</strong> glass were discussed. The effect of various<br />

factors such as pressure, beam gas and working<br />

distance on <strong>the</strong> degree of beam skirting and on<br />

quantitative analysis were also focused.<br />

The poster session continued during <strong>the</strong> tea break.<br />

In <strong>the</strong> last session of <strong>the</strong> day <strong>the</strong> speakers brought<br />

into discussion very distinct topics, such as <strong>the</strong><br />

investigation of medieval opaque glasses and<br />

enamels, analyses of chrome-yellow and chromeorange<br />

dyestuffs used for domestic and imported<br />

cotton fabrics “Touzan” (a vertically stripped Japanese<br />

fabric) in <strong>the</strong> 19 th century, and <strong>the</strong> study<br />

of inscriptions, filing and polishing marks on <strong>the</strong><br />

bronze weapons from <strong>the</strong> Qin Terracotta Army in<br />

China.<br />

The first day ended with a reception at <strong>the</strong> Addis<br />

Gallery, in <strong>the</strong> British Museum.<br />

The second day started with a presentation by<br />

Shirley Northover, focused on <strong>the</strong> application of<br />

electron backscattered diffraction (EBSD) in archaeology.<br />

EBSD patterns are characteristic of <strong>the</strong> structure<br />

and local crystallography orientation of <strong>the</strong><br />

material under <strong>the</strong> beam. By systematically collecting<br />

and analysing <strong>the</strong>se patterns, maps can<br />

be built up revealing <strong>the</strong> distribution of present<br />

phases, showing grain sizes and shapes, and giving<br />

“Quantitative EDX analysis of smalt pigment in <strong>the</strong> variable<br />

pressure SEM”, by Marika Spring.<br />

information on <strong>the</strong> deformation levels of <strong>the</strong> surface.<br />

Hector Lozano spoke on <strong>the</strong> re-discovery of<br />

Mexican fea<strong>the</strong>red textile, a very peculiar technique,<br />

of which only six known textiles still exist,<br />

all of <strong>the</strong>m from <strong>the</strong> 17 th and 18 th centuries. In<br />

this case SEM was used to identify <strong>the</strong> materials<br />

present in <strong>the</strong> fea<strong>the</strong>red yarns particularly <strong>the</strong><br />

identification of <strong>the</strong> birds from which <strong>the</strong> fea<strong>the</strong>rs<br />

were obtained. The next communication was<br />

on <strong>the</strong> study of raw materials used in <strong>the</strong> production<br />

of Chinese porcelain and stoneware bodies,<br />

and <strong>the</strong> last one of <strong>the</strong> session was on <strong>the</strong> role of<br />

SEM-based charcoal identification on reconstructing<br />

vegetation changes in <strong>the</strong> last 40,000 years in<br />

Western Cape (South Africa). The afternoon presentations<br />

were followed by <strong>the</strong> second poster session.<br />

The sixth session began with a presentation from<br />

Diane Johnson on <strong>the</strong> subsurface analysis by application<br />

of a focused ion beam scanning electron<br />

microscope (FIBSEM) to samples of geological<br />

(fossils and meteorites) and historical importance.<br />

Next, Alicia Perea talked on gold usage and<br />

<strong>the</strong> analysis of wear marks and/or deterioration in<br />

site condition of gold artefacts and how difficult<br />

it could be to differentiate one from <strong>the</strong> o<strong>the</strong>r.<br />

Carol Pottasch presented a study on a rediscovered<br />

Dutch painter, Adriaen Coorte (works dating from<br />

10 e-<strong>conservation</strong>


REVIEWS<br />

<strong>16</strong>83-1705) and <strong>the</strong> use of arsenic pigments in his<br />

still lifes. The last presentation – by Eddy Faber -<br />

focused on <strong>the</strong> study of Middle Minoan polychrome<br />

ware production and <strong>the</strong> relations between pottery<br />

production and <strong>the</strong> palaces, and how <strong>the</strong><br />

polychrome ware played an important role in <strong>the</strong><br />

(re)affirmation of both <strong>the</strong> potters and those who<br />

consume <strong>the</strong> craft goods as well as <strong>the</strong> different<br />

strategies for teaching and learning craft skills<br />

in middle Minoan society.<br />

After lunch <strong>the</strong> afternoon began with a communication<br />

on non-invasive sample preparation with<br />

cross-section polishing, followed by a presentation<br />

on <strong>the</strong> Viking filigree, granulation and tool<br />

mark analysis. Next was a presentation by Martina<br />

Raedel on <strong>the</strong> application of environmental<br />

scanning electron microscope (ESEM) equipped<br />

with EDX to <strong>the</strong> study of different types of materials<br />

such as gold mosaics and medieval church<br />

windows, but also to study <strong>the</strong> effectiveness of<br />

corrosion protection systems for historical iron<br />

and cast iron monuments and <strong>the</strong> microbial infestation<br />

of historical marble sculptures. The last<br />

communication focused on <strong>the</strong> study of pre-Columbian<br />

gold beads from Panama and was presented<br />

by Ainslie Harrison. Over 2000 beads were examined,<br />

including 223 beads from recent excavations<br />

in El Caño, from 2008 and 2009 field seasons. All<br />

of <strong>the</strong> beads were examined for type, evidence of<br />

manufacture, alloy composition, fabrications technique<br />

and shape. Specific features of interest,<br />

such as flanges, circumferential grooves, chisel<br />

marks and visible joins, were also noted for each<br />

bead. By correlating <strong>the</strong> analytical data and external<br />

features of <strong>the</strong>se beads, a larger picture of<br />

<strong>the</strong> bead manufacturing processes in pre-Columbian<br />

Panama was revealed.<br />

The conference ended with three presentations.<br />

Aviva Burnstock spoke about The use of SEM imaging<br />

techniques for examination of paintings, showing<br />

examples of <strong>the</strong> application of SEM for questions<br />

related to <strong>the</strong> surface and underlying material<br />

structure of paintings dating from <strong>the</strong> 14 th to <strong>the</strong><br />

20 th centuries. The examples focused in features<br />

such as surface whitening, efflorescence and<br />

changes in <strong>the</strong> surface that resulted from selected<br />

treatments. The second communication entitled<br />

Metallurgy through <strong>the</strong> eyes of <strong>the</strong> SEM, by Nigel<br />

Meeks, illustrated how SEM-EDX has been essential<br />

in revealing <strong>the</strong> materials, metallurgy, construction<br />

and finishing of antiquities, from <strong>the</strong><br />

earliest refining of gold in Lydia, to <strong>the</strong> production<br />

of complex multi-component jewellery in Europe<br />

and to <strong>the</strong> gold metallurgy of Central and<br />

South America. The last presentation was a review<br />

of <strong>the</strong> conference and on <strong>the</strong> future of SEM:<br />

“Current examination of organic remains preserved by metal<br />

corrosion products”, by Andrea Fischer.<br />

A view during <strong>the</strong> poster session.<br />

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REVIEWS<br />

FREE<br />

CONSERVATION<br />

“Inscriptions, filing and polishing marks on <strong>the</strong> bronze<br />

weapons from <strong>the</strong> Qin Terracotta Army in China”, by Xiuzhen<br />

Janice Li.<br />

RESOURCES<br />

SEM 2010, a synopsis and a look to future directions,<br />

by Chris Jones from Hitachi.<br />

During <strong>the</strong> two days conference <strong>the</strong> high standard<br />

on <strong>the</strong> selection of communications and posters<br />

was clear and it was possible to understand how<br />

broad <strong>the</strong> application of SEM and microanalysis<br />

techniques can be. The limitations of <strong>the</strong>se techniques<br />

were addressed as well as <strong>the</strong> progresses<br />

and <strong>the</strong> more recent applications and innovations<br />

in analysis and equipments.<br />

Art Conservation Research<br />

<strong>conservation</strong>research.blogspot.com<br />

Archetype Publications, in association with <strong>the</strong><br />

British Museum, will be publishing <strong>the</strong> conference<br />

proceedings.<br />

ANA BIDARRA<br />

Conservator-restorer<br />

Contact: anabidarra@portugalmail.com<br />

Ana Bidarra has a Degree in Conservation-Restoration<br />

and a Master Degree in GeoSciences on<br />

white structured pigments for restoration. Currently<br />

she is a PhD candidate researching <strong>the</strong><br />

compositional and technological aspects of gold<br />

leaf from Portuguese baroque altarpieces. She<br />

works as conservator-restorer in private practice<br />

since 1999.<br />

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REVIEWS<br />

WESTERN ASSOCIATION FOR ART CONSERVATION (WAAC)<br />

ANNUAL MEETING<br />

Review by Daniel Cull<br />

September 15 - 18, 2010<br />

Portland, Oregon<br />

http://cool.<strong>conservation</strong>-us.org/waac/<br />

The Western Association for Art Conservation<br />

(WAAC) recently held our annual meeting in <strong>the</strong><br />

city of Portland, Oregon. The meeting was sponsored<br />

by <strong>the</strong> University of Oregon (UO), and hosted<br />

by <strong>the</strong> UO White Stag Block, and <strong>the</strong> AIA/Center<br />

for Architecture. The conference was jam packed<br />

with events including: three days of lectures, an<br />

angels project with <strong>the</strong> Oregon Nikkei legacy Center,<br />

a workshop on Digital Imaging Techniques for<br />

Conservation and Education, presented by Cultural<br />

Heritage Imaging, a silent auction to benefit <strong>the</strong><br />

Metropolitan Youth Symphony, a tour of <strong>the</strong> Gamblin<br />

paint factory, and several receptions. There<br />

was barely time to see <strong>the</strong> sights of <strong>the</strong> city, or<br />

<strong>the</strong> Portland Art Museum which had graciously<br />

extended free entry to participants, and of course<br />

Powell's - possibly <strong>the</strong> world’s largest bookshop.<br />

I came away from Portland with a couple of new<br />

books, an awesome notebook from <strong>the</strong> silent auction,<br />

and a few new ideas and techniques to apply<br />

professionally.<br />

After opening addresses and announcements, Dr.<br />

Tami Lasseter-Clare gave <strong>the</strong> first lecture entitled<br />

'Uncovering Mysteries of a Chinese Burial Relic',<br />

demonstrating <strong>the</strong> use of a variety of analytical<br />

techniques (X-radiography, XRF, FTIR) to investigate<br />

<strong>the</strong> originality, and potential dates, of various<br />

parts of a presumed Han dynasty bronze Money<br />

Tree, from <strong>the</strong> collections of <strong>the</strong> Portland Art<br />

Museum. Marie Svoboda gave <strong>the</strong> second lecture<br />

entitled 'Exploring 19 th Century Restorations:<br />

<strong>the</strong> study of Four Apulian Vases from Berlin', this<br />

was one of my favourite lectures, covering an<br />

important topic in <strong>the</strong> <strong>conservation</strong> field; our<br />

own history. The lecture described a collaborative<br />

project between Berlin's Antikensammlung and<br />

LA's J. Paul Getty Museum to study and treat a<br />

group of ceramic artefacts. Part of this study shed<br />

light on <strong>the</strong> original conservator, and it was fun<br />

to see <strong>the</strong> research and experiments that went<br />

into discovering <strong>the</strong> methods and extent of his<br />

work; most intriguing was <strong>the</strong> use of fired clay<br />

blanks as a filling method. The presentation finished<br />

with <strong>the</strong> dilemma now faced by <strong>the</strong> conservators;<br />

to reveal <strong>the</strong> historical artefact or to retain<br />

<strong>the</strong> <strong>conservation</strong> work. I would argue that <strong>the</strong><br />

<strong>conservation</strong> evidence should be retained in at<br />

least some cases.<br />

After <strong>the</strong> break, Chris White gave an excellent<br />

talk on 'Brass and Wood Screws in American Furniture'.<br />

It was interesting to learn about <strong>the</strong> chronology<br />

of screw production as <strong>the</strong>y changed from<br />

all handmade screws prior to 1780 to modern style<br />

screws post 1845, into <strong>the</strong> standardization of<br />

screw in <strong>the</strong> late 19 th and early 20 th centuries.<br />

Chris also announced that Arlen Heginbotham at<br />

<strong>the</strong> Getty is developing an <strong>online</strong> database of<br />

screws and is looking for beta testers. In <strong>the</strong> next<br />

lecture William Hoffman presented 'Silver Tarnishing<br />

Properties of Gloves Used in Conservation',<br />

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REVIEWS<br />

using Oddy testing, Beilstein tests, Azide tests,<br />

as well as FTIR and ATR <strong>the</strong> potential to tarnish<br />

or transfer residue onto silver objects was measured.<br />

The results did not end up with a clear cut<br />

"best choice" glove, but demonstrated instead<br />

that in different ways each of <strong>the</strong> gloves had a<br />

negative effect. The WAAC business meeting was<br />

<strong>the</strong> final point of business prior to lunch.<br />

After lunch Kyle Jansson reviewed <strong>the</strong> current<br />

state of <strong>the</strong> cultural heritage field in a lecture<br />

entitled 'Finding Cures for <strong>the</strong> Common Heritage<br />

Flu'. He presented <strong>the</strong> findings of recent consultations,<br />

unfortunately I think he identified more illnesses<br />

than he did cures! Up next Jan Cavanaugh<br />

discussed 'Art Conservation at <strong>the</strong> Jordon Schnitzer<br />

Mueum of Art', describing how addressing environmental<br />

concerns during an expansion of <strong>the</strong> museum<br />

was required for grants funding to address<br />

<strong>the</strong> long term <strong>conservation</strong> efforts. After <strong>the</strong> break<br />

<strong>the</strong> final round of lectures for <strong>the</strong> day began, with<br />

Anya McDavis-Conway talking about 'The New Mexico<br />

History Museum: Before and After Opening'. I<br />

could totally relate to this, currently being involved<br />

in opening a museum myself. It was interesting<br />

to see <strong>the</strong> storage solutions that had been chosen,<br />

including aluminium pallets to keep objects off of<br />

<strong>the</strong> floor, and purpose built custom saddle mounts.<br />

Yosi Pozeilov’s 'iPad, a New Tool for Condition Reporting<br />

at LACMA', was a fun final lecture for <strong>the</strong><br />

day that outlined how <strong>the</strong> iPad could be utilized as<br />

a tool for <strong>conservation</strong>. Its major bonus is that it<br />

is truly handheld and simulates <strong>the</strong> methods that<br />

we use already.<br />

Yoonjo Lee opened <strong>the</strong> second day with 'Parafilm<br />

M Fills for a Mexican Lacquered Gourd vessel', this<br />

introduced me to an approach that I'd never even<br />

considered - although it was first published by<br />

Marianne Webb in 1998, brilliantly innovative and<br />

strikingly simple, just <strong>the</strong> sort of treatments I most<br />

admire. This was followed by ano<strong>the</strong>r fantastic<br />

The popular 'Crow with LED Eyes' from <strong>the</strong> silent auction<br />

looks out across <strong>the</strong> conference hall.<br />

Photo by Daniel Cull, Some rights reserved.<br />

paper from LACMA, this one entitled 'Nip, Tuck,<br />

and Fill: Producing Digitally Printed Textile Infills<br />

for a Group of Pre-Coumbian Textiles at LACMA',<br />

presented by Lynn Bathke, with a section by Yosi<br />

Pozeilov. During <strong>the</strong> break, examples of <strong>the</strong> printed<br />

fabric and photographs were available, I was<br />

totally excited by this application of photoshop<br />

to <strong>conservation</strong>. The printed fabrics were produced<br />

in collaboration with CadFabulous, an LA based<br />

company using a Mimaki TX4 dye-sublimation<br />

printer, and I can honestly say <strong>the</strong>y looked excellent.<br />

After <strong>the</strong> break, we were treated to two lectures<br />

concerning salt desalination; <strong>the</strong> first, 'Desalination<br />

of Archaeological Ceramics: Measuring Progress<br />

and Success' was presented by Chris White, in<br />

which he presented his work around a normalized<br />

rate equation for calculating <strong>the</strong> relative saltiness<br />

of objects and <strong>the</strong> progress of desalination. He<br />

outlined how current experimental results are<br />

used to define an end point of <strong>the</strong> treatment, at<br />

which an object is declared stable, but that we<br />

still don't have enough results to know what<br />

stable means. In <strong>the</strong> second paper, 'Detecting<br />

and Identifying Testing Salts in Desalination',<br />

Nancy Odegaard discussed <strong>the</strong> use of EM Quant<br />

test strips as a method for semi-quantitative determination<br />

of chlorides, nitrates, and sulfate<br />

14 e-<strong>conservation</strong>


REVIEWS<br />

ions in <strong>the</strong> bath solutions. This appears to be a<br />

cheap and useful analytical method. The last paper<br />

in this session was by Linda Lin who discussed<br />

a 'Technical study and <strong>conservation</strong> of two Japanese<br />

masks: Investigating <strong>the</strong>ir attributes as a pair<br />

and stabilizing fragile matte paint', which treated<br />

us to several examples of <strong>the</strong>se fascinating masks.<br />

After lunch <strong>the</strong>re was one lecture, given by Chris<br />

Stavroudis on 'The Modular Cleaning Program in<br />

Practice Application to Acrylic Paintings', this is<br />

a computer program that assists (but does not<br />

lead) <strong>the</strong> conservator in formulating cleaning<br />

systems. The system was developed as an off shoot<br />

of Richard Wolbers gels cleaning project. I'm led<br />

to believe that <strong>the</strong>se systems are very effective,<br />

but, I have never had cause to use ei<strong>the</strong>r. The<br />

early finish was to allow a brilliant tour, and reception,<br />

at <strong>the</strong> Gamblin paint factory, led by Robert<br />

Gamblin who runs <strong>the</strong> '<strong>conservation</strong> colors'<br />

section of <strong>the</strong> company. It's always fascinating to<br />

see where <strong>the</strong> products we have on <strong>the</strong> shelves in<br />

our labs come from!<br />

The last day of lectures saw a change of venue, and<br />

focus. Art DeMuro began <strong>the</strong> day with 'White Stag<br />

Building Project' a discussion of <strong>the</strong> restoration<br />

of <strong>the</strong> building in which we had spent <strong>the</strong> last<br />

two days. It was fascinating to see how <strong>the</strong> beautiful<br />

building we had been meeting in had previously<br />

been a burnt out shell, <strong>the</strong> previous owner<br />

having attempted to burn it down to claim <strong>the</strong> insurance<br />

money. This project included clever reuses<br />

of unusable parts of <strong>the</strong> building as artwork,<br />

or unique furniture. The second paper of <strong>the</strong> day<br />

'Developing Art and Object Conservation Recommendations<br />

Compatible with Historic Interiors: A<br />

Case Study' was presented by Jil Johnson, and<br />

asked important questions about how we define<br />

Robert Gamblin giving a tour of <strong>the</strong> Gamblin Paint Factory.<br />

Photo by Daniel Cull, Some rights reserved.<br />

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REVIEWS<br />

<strong>the</strong> words we use, such as <strong>conservation</strong> and restoration,<br />

and how <strong>the</strong> different fields may use<br />

<strong>the</strong> same words, but with different emphasis and<br />

meaning. Next up was Tom Fuller who discussed<br />

<strong>the</strong> 'Conservation of Chinese Alters at Kam Wah<br />

Chung & Co.' .This lecture ran over, at <strong>the</strong> request<br />

of <strong>the</strong> audience, and <strong>the</strong>n a discussion ensued.<br />

This site seemed to be a favourite for many attendees,<br />

and <strong>the</strong> presentation was certainly a favourite<br />

of mine, and was probably most in-tune<br />

with <strong>the</strong> ethnographic approaches I most enjoy.<br />

After <strong>the</strong> break Brooke Masek gave a fascinating<br />

lecture entitled 'In Pursuit of <strong>the</strong> Ideal: The Restoration<br />

of <strong>the</strong> Sante-Chapelle', demonstrating<br />

how <strong>the</strong> restoration approach was both led, and<br />

influenced, <strong>the</strong> formation of French national identity.<br />

Exploring <strong>the</strong> 19 th Century ideals of restoration,<br />

and how <strong>the</strong>y were realized, or ignored, in<br />

reality by <strong>the</strong>ir practitioners. This was followed by<br />

Jonathan Fisher's discussion of 'The Putti Project:<br />

Conservation of Two Zinc Fountain Sculptures',<br />

which discussed <strong>the</strong> challenges faced in <strong>the</strong> <strong>conservation</strong><br />

of two sculptures that formed part of a<br />

water feature.<br />

After lunch, Dr. Tami Lasseter-Clare gave ano<strong>the</strong>r<br />

lecture, this time on 'Understanding Performance<br />

Properties and Limitations of Coatings for Metals'.<br />

This was an interesting lecture and raised <strong>the</strong> concern<br />

of how conservators might continue should<br />

products we use be banned, an issue we as a profession<br />

should really be considering more widely.<br />

The next paper was one of <strong>the</strong> most significant,<br />

in my opinion, of <strong>the</strong> whole conference. 'Breaking<br />

Through <strong>the</strong> Glass Ceiling: Exhibiting Art Under<br />

Natural Light at LACMA' was presented by Mark Gilberg,<br />

and co-authored with Charlotte Eng and Frank<br />

Preusser. The lecture presented a case study of <strong>the</strong><br />

successes and failures of a diffused natural lighting<br />

system, in a building designed by renowned<br />

architect Renzo Piano. The authors suggested,<br />

and I agree, that natural lighting is becoming<br />

more common in <strong>the</strong> museum environment, and it<br />

is imperative that conservators begin to share<br />

<strong>the</strong>ir experiences with such lighting systems, and<br />

mitigating <strong>the</strong> worst effects of light damage under<br />

such circumstances. After <strong>the</strong> final break of<br />

<strong>the</strong> conference Mary Slater presented 'Building<br />

as Art: Preserving <strong>the</strong> National Maritime Museum'<br />

which was co-authored by Paul Nachsheim, Jason<br />

Wright, Mark McMillan, Katharine Untch, and<br />

David Wessel, <strong>the</strong> Museum building was originally<br />

designed to look like an Ocean Liner and was a<br />

Works Progress Administration (WPA) project, and<br />

a team of artists decorated it throughout. The<br />

restoration project included both in-situ restoration,<br />

replacement of materials with non-corrosive<br />

but visually similar alternatives, and removal of<br />

parts of <strong>the</strong> building for lab based <strong>conservation</strong>:<br />

a wonderful project, for a wonderful building.<br />

The final paper of <strong>the</strong> conference was 'Conservation<br />

and Beyond: The Fire Restoration of <strong>the</strong> Governor's<br />

Ceremonial Suite in <strong>the</strong> Oregon State Capitol'<br />

by Peter Miejer, this paper discussed <strong>the</strong> collaborative<br />

efforts to conserve this building, working<br />

with conservators, preservation architects,<br />

design architects, owners, insurance representatives,<br />

and not least <strong>the</strong> politicians who would<br />

use <strong>the</strong> building. This paper really highlighted<br />

<strong>the</strong> challenges and achievements of working in a<br />

cross-disciplinary manner that was <strong>the</strong> focus of<br />

this final day.<br />

After three days of papers, and o<strong>the</strong>r activities, <strong>the</strong><br />

conference closed by thanking all <strong>the</strong> presenters,<br />

attendees, and <strong>the</strong> outgoing WAAC President Marie<br />

Laibinis Craft for organizing <strong>the</strong> conference. This<br />

brief review can barely shed light on <strong>the</strong> high<br />

standard of <strong>the</strong> papers, and <strong>the</strong> discussions that<br />

took place. I certainly took some new ideas away<br />

from <strong>the</strong> conference, and that, I think, is <strong>the</strong> litmus<br />

test of a quality conference.<br />

<strong>16</strong> e-<strong>conservation</strong>


NEWS<br />

DEVASTATING FLOOD IN LADAKH, INDIA<br />

A Support Program by Tibet Heritage Fund<br />

By Andre Alexander<br />

Photos by friends of Leh, August 5-7, 2010<br />

On August 5, Ladakh experienced exceptionally<br />

heavy rain, referred to as cloudburst. This triggered<br />

flashfloods and mud slides, hitting lower<br />

Leh, Choklamsar, Sabu, Shey, Basgo, Nyemo, Skorbuchen,<br />

Dhar Hanu and o<strong>the</strong>r villages, causing<br />

untold destruction and so far about 200 confirmed<br />

deaths. More than 200 buildings were completely<br />

destroyed, and fur<strong>the</strong>r 800 were damaged buildings.<br />

According to official count, 1188 households<br />

have been affected across Ladakh. No one can recall<br />

similar heavy rain or a similar catastrophe in<br />

living memory.<br />

Leh's historic old town has not been affected,<br />

and nei<strong>the</strong>r have most temples and monasteries.<br />

Indeed, everywhere it was more recent buildings<br />

and settlements that have been affected, suggesting<br />

that in <strong>the</strong> ancient past, people have been more<br />

careful about where to build. Especially hard hit<br />

was <strong>the</strong> Tibetan refugee settlement at Choglamsar,<br />

established in <strong>the</strong> 1960s.<br />

For over a week, Leh was cut of from <strong>the</strong> rest of<br />

Ladakh, as roads and bridges were also washed<br />

away. There was no electricity and telephony, and<br />

even <strong>the</strong> airport was damaged and closed for one<br />

day. The Indian army quickly rebuilt bridges, cleared<br />

<strong>the</strong> airport runway and <strong>the</strong> major roads. Eventually,<br />

electricity supply and <strong>the</strong> telephone systems<br />

were restored. Many houses were filled to <strong>the</strong><br />

brink with hardening mud. Volunteers from all<br />

sectors of Ladakhi life, Buddhist, Muslims, soldiers,<br />

monks and tourist helped to dig out <strong>the</strong>se<br />

houses, sometimes making terrible discoveries<br />

inside.<br />

Chumikchan Cowshed damage.<br />

Help is coming from abroad and from o<strong>the</strong>r parts<br />

of India, but in an uncoordinated fashion. The<br />

government and Indian donors are building one-<br />

or two-room shelters, from pre-cast concrete slabs<br />

that are brought up. These are not at all suitable to<br />

<strong>the</strong> climate of Ladakh and <strong>the</strong> life-style of its people,<br />

<strong>the</strong> coming winter will be very grim in a concrete<br />

box. Some local Ladakhi NGOs advocate to<br />

build such shelters from concrete-enforced compressed<br />

bricks, but manufacture of such specialized<br />

materials is slow, and winter is approaching.<br />

Detail of damaged modern concrete-frame building at new<br />

bus-stand, Leh.<br />

e-<strong>conservation</strong> 17


NEWS<br />

THF is helping to prevent collapse of damaged<br />

historic buildings in Leh, mainly on <strong>the</strong> edge of<br />

<strong>the</strong> historic old town, and has assessed buildings<br />

for <strong>the</strong>ir safety, advising whe<strong>the</strong>r families can return<br />

to <strong>the</strong>ir houses or not. Certainly, next spring<br />

<strong>the</strong> government and all concerned bodies will have<br />

to take a lot of precautions to prevent <strong>the</strong> catastrophe<br />

from recurring. Most Ladakhis blame <strong>the</strong><br />

climate change, saying historically it has never<br />

rained much in Ladakh (12 th century wall-paintings<br />

in simple buildings with flat mud roofs seem<br />

to bear witness to this). Flood diversion channels<br />

can be built, drainage improved, and protective<br />

walls raised above settlements. Some building<br />

locations may have to be abandoned. But to bring<br />

everyone over <strong>the</strong> winter, THF is proposing an alternative<br />

to building comparatively expensive<br />

shelters (between 2000-4000 Euro) that may not<br />

be suited to <strong>the</strong> local climate, and that may only<br />

be needed for six months.<br />

stay over winter. No expenses for new building materials<br />

are necessary, as everything from a traditional<br />

Ladakhi building can be recycled - including<br />

<strong>the</strong> mud bricks for <strong>the</strong> walls.<br />

Donations to support this program can be sent to:<br />

THF non-profit account in Germany<br />

Account holder: Tibet Heritage Fund<br />

Bank name: Berliner Volksbank<br />

Account Nr. 7104 19 2003<br />

BLZ 100 900 00<br />

SWIFT/BIC BEVODEBB<br />

IBAN: DE03 1009 0000 7104 1920 03<br />

We found that it only takes two skilled masons and<br />

some helpers to make at least one room in each<br />

of <strong>the</strong> damaged buildings safe for <strong>the</strong> family to<br />

Volunteers at work cleaning <strong>the</strong> debris from <strong>the</strong> new<br />

bus-stand area.<br />

Panoramic view of <strong>the</strong> damage suffered at lower Leh from <strong>the</strong> mudslide.<br />

18<br />

e-<strong>conservation</strong>


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EVENTS<br />

November 2010<br />

NODEM10<br />

Nordic Digital Excellence in Museums<br />

From Place to Presence. Digital media breaking boundaries<br />

between inside, outside and virtual spaces, in heritage<br />

institutions<br />

Date: 24-26 November<br />

Read more...<br />

7 th International Conference on Science<br />

and Technology in Archaeology and<br />

Conservation<br />

And <strong>the</strong> Workshop on Documentation and Conservation of<br />

Stone Deterioration in Heritage Places<br />

Date: 7-12 December<br />

Read more...<br />

December 2010<br />

Place: Copenhagen, Denmark<br />

Place: Petra, Jordan<br />

NODEM is a bi-annual conference that explores <strong>the</strong> role<br />

The Workshop will focus on documentation and conserva-<br />

of digital media in museums. One of <strong>the</strong> most striking<br />

tion of stone. Organized jointly with by <strong>the</strong> ICOMOS Sci-<br />

features of digital media in museums today is <strong>the</strong>ir po-<br />

entific Committees of Heritage Documentation (CIPA,<br />

tential for linking and integrating resources, spaces and<br />

Stone Committee (ISCS), and ICAHM) <strong>the</strong> workshop is<br />

users in an abundance of ways. Museums can share con-<br />

aimed at ga<strong>the</strong>ring a multidisciplinary group of heritage<br />

tent and gain exposure as well as work across <strong>online</strong> and<br />

documentation and <strong>conservation</strong> specialists around <strong>the</strong><br />

onsite, users can contribute to knowledge production<br />

issue of <strong>the</strong> use of advanced recording techniques for<br />

and choose between different exhibition platforms, and<br />

identifying, maping, and understanding wea<strong>the</strong>ring<br />

experiences and knowledge can be mediated through a<br />

forms and processes affecting <strong>the</strong> significance and<br />

variety of channels.<br />

integrity of cultural heritage surfaces.<br />

Works of Art and Conservation Science<br />

Today<br />

Date: 26-28 November<br />

Read more...<br />

CALL FOR PAPERS: 2 nd International<br />

Conference on Salt Wea<strong>the</strong>ring<br />

of Buildings and Stone Sculptures<br />

Place: Thessaloniki, Greece<br />

Date: 24-25 Septembe<br />

Read more...<br />

Place: Austin, Texas, USA<br />

The central aim of <strong>the</strong> Symposium is to bring toge<strong>the</strong>r<br />

renowned scientists and experts from all over <strong>the</strong><br />

The conference organised by <strong>the</strong> Building Materials La-<br />

world, who will present <strong>the</strong> state-of-<strong>the</strong>-art in<br />

boratory of <strong>the</strong> University of Cyprus follows a very suc-<br />

<strong>conservation</strong> science and practice, and exchange views<br />

cessful first meeting that was held in Copenhagen, Den-<br />

on key issues related to <strong>the</strong> preservation of our cultural<br />

mark in October 2008. It will take place in Limassol, at<br />

heritage. The Symposium will address major fields of<br />

<strong>the</strong> newly renovated 5-star Grand Resort, between 19-22<br />

<strong>conservation</strong> science including modern diagnostic<br />

October 2011. The meeting is open to both practitioners<br />

techniques, materials for <strong>conservation</strong>, paintings,<br />

and researchers and it is anticipated to address general<br />

metals and ceramics, pigments and dyes, textiles,<br />

salt-related problems and decay mechanisms, <strong>the</strong> key<br />

wood, paper and manuscripts. Basic <strong>the</strong>me in one of<br />

parameters controlling salt crystallisation and new con-<br />

<strong>the</strong> main panels will be <strong>the</strong> Education/Curriculum of<br />

servation approaches and materials.<br />

Conservation Science today.<br />

The symposium will be held in <strong>the</strong> facilities of Byzantine<br />

The deadline for abstract submission is 17 December 2010.<br />

Culture and Archaeological museums and <strong>the</strong> University<br />

For more information, please visit <strong>the</strong> conference web-<br />

Ecclesiastical Academy, according to <strong>the</strong> program.<br />

site or send an email to swbss@ucy.ac.cy.<br />

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e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

AND COMPARISON TO<br />

IVORY PORTRAIT MINIATURES<br />

by Josie Wornoff<br />

Ivory has been used in <strong>the</strong> creation of objects since <strong>the</strong> beginning of civilization, due to its prized<br />

durability and appearance. Early uses included weaponry, musical instruments, religious pieces,<br />

personal artifacts, decorative items, artistic pieces, and occasionally, book covers. Three small books<br />

from <strong>the</strong> Library and Archives Canada study collection were suspected to have ivory covers. Various<br />

identification tests were administered on <strong>the</strong> book covers, and Fourier Transform Infrared Spectroscopy<br />

analysis confirmed <strong>the</strong>ir elephant ivory composition. However, related literature and o<strong>the</strong>r existing<br />

examples of ivory covered books are rare. In contrast, <strong>the</strong> use of ivory in portrait miniatures is<br />

extensively researched. Library and Archives Canada has over 130 portrait miniatures, and has<br />

successfully treated many of <strong>the</strong>se. Comparison between <strong>the</strong> history, processing, and risks of<br />

deterioration of <strong>the</strong>se two applications of ivory revealed many similarities. From this, similar<br />

<strong>conservation</strong> techniques of portrait miniatures are proposed for use on ivory book covers.


IDENTIFICATION OF IVORY BOOK COVERS<br />

Introduction<br />

Identification of Ivory<br />

The cover material of four small books (Figure 1)<br />

was <strong>the</strong> subject of a research project at Library<br />

and Archives Canada (LAC). Three of <strong>the</strong> books<br />

appeared to be produced of ivory or an ivory substitute,<br />

and <strong>the</strong> fourth resembled tortoiseshell or<br />

horn. Information was ga<strong>the</strong>red on <strong>the</strong> history<br />

and characteristics of ivory and ivory substitutes,<br />

while identification tests were administered to<br />

determine <strong>the</strong> exact compositions of <strong>the</strong> book<br />

covers.<br />

Extensive research revealed that <strong>the</strong>re is very<br />

little mention of ivory book covers in literature.<br />

Though <strong>the</strong>se ivory book covers are quite rare,<br />

<strong>the</strong>re are currently over 130 portrait miniatures<br />

in <strong>the</strong> LAC collection. Since <strong>the</strong> history of ivory<br />

use, ivory processing, and risks of deterioration<br />

are very similar between ivory book covers and<br />

ivory portrait miniatures, similar <strong>conservation</strong><br />

recommendations are proposed for use on ivory<br />

book covers.<br />

There are many methods of testing for ivory, yet<br />

<strong>the</strong>re is no test that is reliable, simple, and inexpensive<br />

[1]. In fact, reliability is limited because<br />

most tests can only prove that a substance is not<br />

ivory, and cannot avoid a destructive aspect in<br />

order to provide this diagnosis [1].<br />

Testing methods<br />

Preliminary examination revealed certain morphological<br />

characteristics that aided in material<br />

identification. For example, <strong>the</strong> size of <strong>the</strong> covers<br />

indicated that <strong>the</strong>y could not be composed of<br />

smaller proteinaceous materials such as antler<br />

or horn [2]. Photography under various lighting<br />

conditions also revealed important details, such<br />

as ivory grain patterns under transmitted light.<br />

Lamellae grain patterns are present in longitudinal<br />

cuts in ivory tusks, whereas Lines of Shreger<br />

are present in cross-sections which provide distinction<br />

from mammoth ivory [1].<br />

Figure 1. For referral purposes, from left to right: Book 3, Book 1, Book 2, and Book 4.<br />

e-<strong>conservation</strong><br />

25


JOSIE WORNOFF<br />

Figure 2. Ivory fluorescence during ultraviolet light testing.<br />

Ultraviolet light was also used to distinguish bluepurple<br />

fluorescing ivory [3], from darker and dull<br />

syn<strong>the</strong>tic materials [4]. The three small ivory<br />

books each fluoresced a bright colour, while <strong>the</strong><br />

added resins revealed a green colour. Book 4 fluoresced<br />

a dull, mottled colour, but identification<br />

guidelines for tortoiseshell or horn were inconclusive<br />

(Figure 2).<br />

Figure 3. Hot needle test on Book 4.<br />

Many polymer imitations of ivory will melt or burn<br />

under heated conditions [3]. A hot needle was<br />

applied to <strong>the</strong> surface of each cover, leaving only<br />

a small black dot on <strong>the</strong> first three books, indicating<br />

true ivory [4]. However, Book 4 became<br />

very soft with heat, and <strong>the</strong> needle entered readily,<br />

disfiguring <strong>the</strong> surface (Figure 3). Similarly,<br />

a small shaving of each book cover was held in a<br />

flame to perform a burn test. A shaving of celluloid<br />

or o<strong>the</strong>r substitute will burn rapidly and completely,<br />

often releasing <strong>the</strong> odor of camphor which<br />

was used to increase strength and decrease flammability<br />

of cellulose nitrate [5]. The shaving of <strong>the</strong><br />

ivory substances smelled vaguely of bone, but <strong>the</strong><br />

odour of <strong>the</strong> brown book was distinctively burning<br />

plastic.<br />

A chemical test that would have been more conclusive<br />

is <strong>the</strong> diphenylamine spot test. A blue-violet<br />

stain will appear within seconds if cellulose nitrate<br />

Figure 4. FT-IR spectroscopy testing at CCI on Book 1.<br />

26 e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

is present, and any o<strong>the</strong>r colour or no colour change<br />

indicates cellulose nitrate is not present [6]. This<br />

test would have been successful in determining<br />

that <strong>the</strong> brown book was in fact cellulose nitrate,<br />

but not aid in identifying <strong>the</strong> o<strong>the</strong>r books.<br />

Scientific Analysis<br />

Finally, a conclusive test was administered. Scott<br />

Williams, Senior Conservation Scientist at <strong>the</strong> Canadian<br />

Conservation Institute (CCI), performed<br />

Fourier Transform Near Infrared Reflectance Spectroscopy<br />

testing on <strong>the</strong> four books as well as an<br />

elephant ivory sample [7] (Figure 4). A LabSpec<br />

Pro NIR spectrometer (Analytical Spectral Devices)<br />

with a bifurcated fibre optic reflection probe was<br />

used to ga<strong>the</strong>r spectra from each material [7]. The<br />

characterization of <strong>the</strong> material is determined by<br />

its molecular interaction with <strong>the</strong> infrared radiation<br />

which originates a characteristic spectrum<br />

[8].The spectra were <strong>the</strong>n arranged on graphs in<br />

comparison with <strong>the</strong> spectra of reference materials<br />

of known compositions [7].<br />

From <strong>the</strong> ga<strong>the</strong>red spectra, it is evident that Book<br />

1, Book 2 and Book 3 are each pure elephant ivory<br />

(Figure 5). Every spectrum of each book (except<br />

Book 4) is very closely related to <strong>the</strong> sample spectra<br />

of a known elephant tusk. However, Book 4 did<br />

not closely compare to <strong>the</strong> elephant tusk sample<br />

at all. However, it did relate closely to sample spectra<br />

from cellulose nitrate (Figure 6) Therefore, it<br />

was concluded with certainty that Book 1, Book 2,<br />

and Book 3 are made of true elephant ivory, and<br />

Book 4 is made of cellulose nitrate.<br />

History of Ivory Use<br />

Early man utilized as much of mammoths as possible,<br />

beginning <strong>the</strong> tradition of ivory use in both<br />

utilitarian and decorative objects [3]. Early uses<br />

included weaponry, musical instruments, religious<br />

pieces, personal artifacts, decorative items, artistic<br />

pieces, and parts for games [3]. Ivory became associated<br />

with gold and silver as a luxurious commodity,<br />

used especially for decorating objects of<br />

value [1].<br />

Figure 5. Spectra of Book 1, Book 2, and Book 3 compared to sample ivory (red) (Graph: Scott Williams).<br />

Covers and embellishments for all books<br />

have spectra similar to elephant ivory<br />

(red trace).<br />

e-<strong>conservation</strong><br />

27


JOSIE WORNOFF<br />

The spectra of <strong>the</strong> cover and cross are nearly<br />

identical to each o<strong>the</strong>r and to that of a reference<br />

sample of cellulose nitrate (red trace), but differ<br />

from ivory (grey trace) and tortoiseshell (pink<br />

trace). Cellulose nitrate was commonly used<br />

to simulate tortoiseshell.<br />

Figure 6. Spectra of Book 4 compared to cellulose nitrate (red) and ivory (grey) (Graph: Scott Williams).<br />

Along with its ability to outlast o<strong>the</strong>r common materials<br />

such as paper, cloth, and wood, ivory is<br />

also prized for its clean beauty, smoothness, and<br />

ability to show a bright gloss [1]. The ivory book<br />

covers feature <strong>the</strong>se aes<strong>the</strong>tic qualities, but <strong>the</strong><br />

relatively good condition indicates that <strong>the</strong>y were<br />

likely on display as revered religious objects in<br />

accordance with historical fashionable use.<br />

Ivory Use in Book Covers<br />

The use of ivory in book covers has rarely been focused<br />

on in <strong>the</strong> past; however, it is occasionally<br />

mentioned in literature regarding general ivory<br />

use. The three books are each comprised of two<br />

pieces of thin ivory to serve as book covers, and<br />

on Book 2, a third piece for a spine. However, a<br />

more common practice throughout history was<br />

to repurpose two plaques or <strong>the</strong> two pieces of a<br />

diptych to enclose written material.<br />

An early use of ivory books is mentioned in <strong>the</strong> 275<br />

C.E. Roman history Scriptores Historiae Augustae<br />

[9]. Ivory panels were used to record names and<br />

deeds of emperors, which was a tradition that extended<br />

to <strong>the</strong> later Roman and Byzantine courts.<br />

This confirms <strong>the</strong> continued early use of ivory<br />

books on ceremonial occasions, and indicates<br />

that <strong>the</strong> book format was likely two tablets hinged<br />

toge<strong>the</strong>r.<br />

In <strong>the</strong> Early Middle Ages, ivory continued to be<br />

highly revered and was used sparingly for important<br />

commissions, which included <strong>the</strong> covers of<br />

imperial manuscripts [10]. Many of <strong>the</strong> ivory objects<br />

made in <strong>the</strong> Late Roman and Early Medieval<br />

periods, including consular diptychs and ivory<br />

book covers, have survived above ground to <strong>the</strong><br />

present day. This unique preservation is due to a<br />

combination of <strong>the</strong> material’s durability and <strong>the</strong><br />

traditions sanctioned by church and state throughout<br />

history [10].<br />

In addition to ceremonial recognition and imperial<br />

documentation, ivory was very commonly used to<br />

emphasize <strong>the</strong> importance of religious imagery<br />

28 e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

and texts. The Carolingian period marked a revival<br />

of ivory carving [10], particularly in ecclesiastical<br />

furniture, reliquaries, and book covers [1]. Charlemagne<br />

sought to recreate <strong>the</strong> glory and culture of<br />

ancient civilizations by having scribes and artists<br />

copy classical texts and illustrations, including<br />

many books of lavish miniatures and gold and/or<br />

ivory covers [10]. After <strong>the</strong> Carolingian revival,<br />

ivory continued to be used for making fine book<br />

covers for treatises of special merit or religious<br />

manuscripts [1].<br />

A less figurative and more decorative design became<br />

more common in <strong>the</strong> later years. This is more<br />

representative of <strong>the</strong> simple, elegant designs of<br />

<strong>the</strong> three deaccessioned books, as <strong>the</strong>y are from<br />

<strong>the</strong> late 19 th century. Book 1 has four fleur-de-lis<br />

additions on <strong>the</strong> front and back, and an ink emblem<br />

on <strong>the</strong> center medallion. Book 2 has a simple<br />

yet beautiful oval medallion and surrounding engraving,<br />

while Book 3 includes an asymmetrical<br />

center addition.<br />

Ivory Use in Portrait Miniatures<br />

books, so miniaturists continued to illustrate books<br />

but also offered patrons independent miniatures<br />

[11]. In <strong>the</strong> 1520s, individual portraits in miniature<br />

size were first produced at French and English<br />

courts on a portable piece of parchment or<br />

vellum [11]. This transfer of art technique relied<br />

on an understanding of <strong>the</strong> close association between<br />

<strong>the</strong> materials and techniques of <strong>the</strong> illuminated<br />

book and <strong>the</strong> early miniature on parchment<br />

[12]. It is interesting to consider <strong>the</strong> implication<br />

on portrait miniatures had an early ivory book been<br />

present and considered for <strong>the</strong> same transfer of<br />

application.<br />

Instead, small scale portrait images were painted<br />

in a range of materials, styles, and techniques,<br />

from water-based paints on paper or card supports,<br />

to fired enamels on gold or copper supports, and<br />

oil paints on metal, stone, glass and tortoiseshell<br />

[12]. However, <strong>the</strong> most significant early methods<br />

of painting portraits were on parchment or vellum,<br />

called limnings, becoming known as portrait miniatures<br />

in <strong>the</strong> 18 th century when <strong>the</strong>y began to be<br />

painted on ivory [12].<br />

The use of ivory in books seems to have not experienced<br />

a specific period of use, but ra<strong>the</strong>r was in<br />

use periodically throughout history. In contrast,<br />

portrait miniatures were very popular during a<br />

400 year time period. Both ivory objects are intended<br />

to show a kind of devotion; <strong>the</strong>se particular<br />

books to display religious beliefs, and <strong>the</strong> portrait<br />

miniatures to commemorate a loved one or<br />

important figure. The books were likely on display<br />

in a home when <strong>the</strong>y were not in use as a Catholic<br />

missal to celebrate Mass throughout <strong>the</strong> year, however,<br />

<strong>the</strong> miniatures were often more personal than<br />

for display.<br />

Notably, early portrait miniatures were derived<br />

from illuminated manuscripts. From <strong>the</strong> 1460s,<br />

handwritten books had to compete with printed<br />

The first watercolour portraits on ivory tablets<br />

were attributed to <strong>the</strong> Venetian artist Rosalba<br />

Carriera [13]. These were initially used as bases<br />

or lids for boxes [13], much like <strong>the</strong> repurposing<br />

of diptychs and plaques for early ivory books.<br />

Carriera ga<strong>the</strong>red fame throughout Europe for<br />

<strong>the</strong> beauty of <strong>the</strong> ivory visible through <strong>the</strong> transparent<br />

paint in flesh coloured areas [13]. By 1710,<br />

artists internationally faced pressure to conform<br />

to this new fashion despite <strong>the</strong> difficulty of painting<br />

watercolour on <strong>the</strong> unabsorbent ivory [13].<br />

After <strong>the</strong> introduction of ivory as a support for portrait<br />

miniatures, parchment use began to decline<br />

until it stopped entirely [12]. The popularity of <strong>the</strong><br />

portrait miniature was decreasing by 1839 with <strong>the</strong><br />

introduction of <strong>the</strong> daguerreotype, a few decades<br />

e-<strong>conservation</strong><br />

29


JOSIE WORNOFF<br />

before <strong>the</strong>se books were produced in Europe. However,<br />

it is likely that <strong>the</strong> materials and techniques<br />

from portrait miniatures remained readily available<br />

to adapt to <strong>the</strong> production of <strong>the</strong>se ivory<br />

book covers.<br />

Ivory Processing<br />

Due to <strong>the</strong> lack of published information on ivory<br />

books, it is only possible to infer how <strong>the</strong> covers<br />

were formed. However, <strong>the</strong>re are many resources<br />

on <strong>the</strong> general processing of ivory, as well as techniques<br />

used to make ivory leaves for miniatures.<br />

First <strong>the</strong> brownish outer bark-like layer is removed<br />

[1], followed by <strong>the</strong> seasoning, cutting, smoothing,<br />

and forming of ivory into a sheet.<br />

Ivory is hygroscopic, like wood [14]. Therefore,<br />

seasoning is required to allow for natural shrinkage;<br />

weight losses of up to 4% have been recorded<br />

[1]. Without controlled drying, ivory will likely<br />

crack or warp [15]. However, it is an o<strong>the</strong>rwise<br />

ideal material to process due to its dense, virtually<br />

grainless and evenly textured nature [10].<br />

Many tools and techniques have been used to cut<br />

ivory throughout history. Many cutting and carving<br />

tools were employed, including: saws, shears,<br />

rasps, files, drills, punches, chisels, picks, scrapers,<br />

and a variety of knives and similar cutting instruments.<br />

For flat sections, <strong>the</strong> broad surfaces were<br />

cut radially to show <strong>the</strong> edges of <strong>the</strong> ivory’s lamellae,<br />

or tangentially to create a finer looking ivory<br />

with less noticeable grain [15].<br />

During <strong>the</strong> popularity of portrait miniatures, ivory<br />

sheets were available for purchase in pre-cut sheets<br />

called leaves [<strong>16</strong>]. These leaves were cut lengthwise<br />

from <strong>the</strong> elephant’s tusk [<strong>16</strong>]. The ivory book<br />

covers are each around 1 mm thick, slightly thicker<br />

than most portrait miniature leaves, yet quite<br />

similar (Figures 7 and 8).<br />

Figure 7. Verso of a portrait miniature revealing <strong>the</strong> longitudinal<br />

lamellae of ivory.<br />

Figure 8. Characteristic ivory longitudinal grain patterns in<br />

Book 1.<br />

Figures 6-8. Sampling in Coptic fragments codes from <strong>the</strong><br />

National Archaeological Museum. From up to down: 15064;<br />

15065 and 1976/130/11. Photos by José Baztan.<br />

30 e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

Ancient carvers managed to hand cut ivory into<br />

a thin veneer cylinder, which was cut into pieces<br />

and subsequently softened and mounted upon <strong>the</strong><br />

curved faces and hands of sculptures [1]. Medieval<br />

book covers may have been made this way as <strong>the</strong>re<br />

are some early surviving ivory book covers as large<br />

as 30 cm square [1].<br />

The size of leaves was limited by <strong>the</strong> diameter of<br />

tusks, until technology developed for <strong>the</strong> production<br />

of larger sheets of ivory in <strong>the</strong> early 19 th century<br />

[<strong>16</strong>]. Ivory was spiral cut with a reciprocating<br />

saw into a scroll, steamed until soft, <strong>the</strong>n subjected<br />

to hydraulic pressure to flatten to a desired size<br />

[<strong>16</strong>]. The resulting ivory had an increased flexibility,<br />

a finer polish, and less grain patterns [17], but <strong>the</strong><br />

surface was often wavy and needed to be laid down<br />

on stiff card before painting could begin [<strong>16</strong>].<br />

Miniaturists were traditionally concerned about<br />

<strong>the</strong> permanence and stability of <strong>the</strong>ir ivory leaves<br />

[<strong>16</strong>]. Veneer cut ivory proved undesirable as <strong>the</strong><br />

ivory was prone to shattering into thin, parallel<br />

segments [<strong>16</strong>]. Therefore, miniaturists continued<br />

to cut leaves in <strong>the</strong> traditional manner, just as <strong>the</strong>y<br />

continued to use <strong>the</strong> same materials and techniques<br />

since <strong>the</strong> 18 th century [<strong>16</strong>]. Since watercolour paint<br />

did not readily adhere to <strong>the</strong> ivory material, miniature<br />

leaves required <strong>the</strong> extra steps of degreasing,<br />

whitening, and scraping [18].<br />

Risks for Deterioration of Ivory<br />

The most common instances of ivory deterioration<br />

are warping, cracking and complications arising<br />

from added materials. Ivory is a relatively stable<br />

material, but only in a constant environment [19].<br />

It is an anisotropic material, and is <strong>the</strong>refore susceptive<br />

to warping and cracking on exposure to<br />

heat or moisture [3]. Thin artifacts such as miniatures<br />

and book covers are especially vulnerable,<br />

as even moisture and heat from hands may be<br />

damaging [3].<br />

Warping<br />

The risk of warping is increased when <strong>the</strong> ivory is<br />

mounted on stiff backing cards, restricting natural<br />

Figure 9. Severe warp of a portrait miniature at LAC.<br />

e-<strong>conservation</strong><br />

31


JOSIE WORNOFF<br />

movement [12]. Ivory should be allowed to expand<br />

or contract with changes in temperature, which<br />

will be at a different rate than of <strong>the</strong> paper [1]. The<br />

front of <strong>the</strong> ivory sheet shrinks laterally, while <strong>the</strong><br />

back is restrained by <strong>the</strong> glue and paper [20]. Warping<br />

often occurs parallel to <strong>the</strong> grain [20] in an<br />

even, concave curvature [21].<br />

Many miniatures have a slight warp, but it is often<br />

considered acceptable if it is not too extreme [21]<br />

(Figure 9). The ivory covers on Book 2 are moderately<br />

warped, similar to portrait miniatures with<br />

restricting backing cards (Figure 10). A sign of<br />

unstable warping is irregular buckling caused by<br />

stresses between <strong>the</strong> ivory and an unevenly attaching<br />

backing [21]. This will eventually cause<br />

cracking and splitting [1].<br />

Cracking<br />

Often <strong>the</strong>re is insufficient room within <strong>the</strong> frame<br />

of a miniature to allow <strong>the</strong> ivory to react to atmospheric<br />

conditions, causing <strong>the</strong> ivory to warp and<br />

crack [22]. This is seen on Book 3, as <strong>the</strong> metal<br />

casing is restricting movement of <strong>the</strong> ivory book<br />

covers, worsening <strong>the</strong> warp into a more uneven,<br />

unstable buckling. The fabrication of <strong>the</strong>se three<br />

books is inherently faulty, as <strong>the</strong> covers cannot<br />

stay adhered to <strong>the</strong> board as well as clasped for a<br />

long amount of time. Ei<strong>the</strong>r <strong>the</strong> ivory piece lifts<br />

from <strong>the</strong> front cover and stays clasped, or <strong>the</strong> ivory<br />

stays attached but <strong>the</strong> clasp breaks off. This is<br />

evident on Book 1 and Book 2, respectively (Figure<br />

11).<br />

Added materials<br />

Ivory book covers are essentially a combination of<br />

materials, so <strong>the</strong>re are often anticipated problems<br />

with added materials. Metals provide a great aes<strong>the</strong>tic<br />

contrast with ivory; however, <strong>the</strong> materials<br />

react differently to environmental conditions. Sudden<br />

changes in temperature expand metal more<br />

than <strong>the</strong> brittle ivory, putting an undue mechanical<br />

pressure on <strong>the</strong> area [4]. Galvanic currents<br />

are formed between materials with diverse elec-<br />

Figure 10. Moderate warp of Book 2.<br />

32 e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

Figure 11. The completely detached ivory cover of Book 1.<br />

trical potential, which weakens <strong>the</strong> ivory creating<br />

cracks [4]. This often occurs at <strong>the</strong> point of contact<br />

between <strong>the</strong> ivory and <strong>the</strong> metal, as seen in<br />

Book 3 where cracks have occurred and Book 2 has<br />

even broken off into pieces at <strong>the</strong> areas in contact<br />

with <strong>the</strong> metal hinges (Figure 12).<br />

<strong>the</strong> ivory book covers is similar to that of portrait<br />

miniatures and more general ivory objects. Treatments<br />

for portrait miniatures may be adapted to<br />

ivory book covers, specifically focused on basic<br />

cleaning, minimizing warp, and repairing cracks<br />

and losses.<br />

Paint films suffer crazing, cracking and peeling<br />

due to improper preparation of <strong>the</strong> paint or <strong>the</strong><br />

ivory support [12]. Watercolour paint is very susceptible<br />

to any moisture, including relative humidity,<br />

cleaning solutions, and general water staining<br />

[12]. None of <strong>the</strong> books have painting on <strong>the</strong>m,<br />

though Book 1 has an intricate ink design on <strong>the</strong><br />

center medallion.<br />

Figure 12. The broken edge on Book 2 due to stress of previous<br />

clasp.<br />

Conservation<br />

The unique problems associated with ivory require<br />

specialized <strong>conservation</strong>. Much of <strong>the</strong> damage on<br />

e-<strong>conservation</strong><br />

33


JOSIE WORNOFF<br />

Cleaning<br />

Basic cleaning of portrait miniatures should be<br />

done with a soft brush, cloth, or lea<strong>the</strong>r [21].<br />

Water and mild soap cannot be applied on thin films<br />

of ivory as <strong>the</strong>y are particularly susceptible to<br />

water damage [3] and may cause condensation,<br />

water damage, or mould [12]. The ivory is quite<br />

dirty on all three books, especially in recessed areas.<br />

Dry clean methods such as a stiff brush should be<br />

used to enter all depressions to remove surface<br />

dirt while leaving <strong>the</strong> natural patina. A dry, soft<br />

cloth may also be used to rub <strong>the</strong> exterior to extract<br />

<strong>the</strong> natural oils of <strong>the</strong> ivory.<br />

The preservation of original frames and cases are<br />

an important aspect of <strong>the</strong> <strong>conservation</strong> of miniature<br />

portraits. If a frame requires cleaning, a<br />

damp swab may be applied locally after removal<br />

of miniature, or it may be polished with a soft<br />

flannel cloth or Hagerty Jewelry Cloth [23]. The<br />

metal clasps on Book 1 and Book 3 and <strong>the</strong> frame<br />

on Book 3 may benefit from polishing with <strong>the</strong>se<br />

techniques.<br />

Aged ivory develops a yellowish patina which is<br />

natural to <strong>the</strong> object and should not be removed<br />

[14]. However, removal of water stains and aged<br />

varnish may be desired for aes<strong>the</strong>tic purposes on<br />

portrait miniatures. Acetone may be used to dissolve<br />

aged adhesive or varnish, and a scalpel to<br />

mechanically remove <strong>the</strong> rest [23]. The appearance<br />

of water damage can be minimized by coloured<br />

pencils [23]. Book 3 appears to have a discoloured<br />

Figure 13. Adhesive staining overall on Book 3.<br />

34 e-<strong>conservation</strong>


IDENTIFICATION OF IVORY BOOK COVERS<br />

varnish applied over <strong>the</strong> ivory, distracting from <strong>the</strong><br />

natural beauty of <strong>the</strong> underlying ivory. Acetone<br />

swab could be used to remove varnish, however it<br />

is likely too risky to attempt removal of <strong>the</strong> varnish<br />

as <strong>the</strong> ivory is inset into <strong>the</strong> metal frames<br />

(Figure 13).<br />

Warping<br />

The removal of backings from portrait miniatures<br />

often reduces <strong>the</strong> pressure that is causing <strong>the</strong>m<br />

to warp [24]. Miniatures are placed face down<br />

and a thin scalpel blade is used to peel away <strong>the</strong><br />

backing, ensuring it is secure on a curved support.<br />

Adhesives may require softening with a damp blotter<br />

[23], less than 50% ethanol in water [20], or<br />

10% Laponite solution through a tissue [23]. In<br />

miniatures, <strong>the</strong> backing cards are an addition to<br />

facilitate painting of <strong>the</strong> ivory. In books, <strong>the</strong> backings<br />

are <strong>the</strong> book board, an integral part of <strong>the</strong><br />

structure and intention of <strong>the</strong> object. Thus despite<br />

warping, it is not advisable to remove <strong>the</strong><br />

ivory from <strong>the</strong> card, nor reline <strong>the</strong> ivory.<br />

The warping of ivory is a serious issue for portrait<br />

miniatures as it affects <strong>the</strong> delicate paint layer and<br />

may escalate until <strong>the</strong> ivory exceed <strong>the</strong> dimensions<br />

of its case [22]. Ivory pieces can be placed in a<br />

chamber conditioned with silica gel at 65-70%<br />

RH for 10 minutes up to 2-5 hours, <strong>the</strong>n clamped<br />

between Plexiglas ® sheets [23]. This successfully<br />

relaxes ivory to a more flattened state.<br />

In addition, a Gore-Tex ® humidifying system has<br />

been adapted from paper <strong>conservation</strong> to flatten<br />

miniatures on ivory [24]. The miniature is placed<br />

concave side down, between layers of Gore-Tex ® ,<br />

silicon paper, blotting paper, and plastic [25]. Gore-<br />

Tex ® allows a controlled amount of moisture to<br />

pass through <strong>the</strong> ivory, and if necessary, increased<br />

weighting will gradually flatten <strong>the</strong> ivory in 4-8<br />

hours [26].<br />

Though <strong>the</strong> silica gel and Gore-Tex ® methods do<br />

reduce irregular distortions, it is often not possible<br />

or wise to attempt to completely flatten <strong>the</strong><br />

miniature [24]. A safe alternative to attempting<br />

to force <strong>the</strong> ivory flat is simply to accept some<br />

distortion [24]. In fact, specialized sink mats can<br />

be made with 2-ply rag board [23] or Plastazone,<br />

which allow responses to changes in environment<br />

from <strong>the</strong> portrait miniatures [24].<br />

Though <strong>the</strong>re is a significant warp in <strong>the</strong> ivory of<br />

<strong>the</strong>se books, flattening treatment is not recommended.<br />

There are too many mixed materials in<br />

<strong>the</strong> books to attempt flattening. Each of <strong>the</strong>se<br />

materials would respond differently to <strong>the</strong> moisture<br />

introduced in flattening treatments. Fur<strong>the</strong>rmore,<br />

Book 1 and Book 2 exhibit natural curving<br />

which do not conform to <strong>the</strong> text block, nor should<br />

it be forced. Book 3 shows restrained buckling<br />

that is caused by various pressures exerted from<br />

<strong>the</strong> metal framing, adhesive and varnish. If <strong>the</strong>se<br />

pieces were detached, <strong>the</strong>y would benefit from a<br />

relaxing treatment from ei<strong>the</strong>r silica gel chamber<br />

or a Gore-Tex® procedure.<br />

Cracking<br />

Ivory cracks and losses are <strong>the</strong> result of former<br />

stresses and distortions, meaning pieces may not<br />

align and will be difficult to successfully repair<br />

[19]. Thus, <strong>the</strong>y should be treated in <strong>the</strong> early<br />

stages as soon as possible to avoid increased damage<br />

[24]. Unfortunately, very extreme warping<br />

and cracking of ivory is essentially irreversible [3].<br />

Prior to treatment of ivory cracks, individual pieces<br />

must be flattened first [20], with <strong>the</strong> backing paper<br />

removed [24].<br />

Experimentation to find <strong>the</strong> ideal adhesive for<br />

treating ivory resulted in nearly every material<br />

being used in <strong>the</strong> past [27]. Mowilith DMC2 is<br />

currently recommended based on CCI test results,<br />

e-<strong>conservation</strong><br />

35


IDENTIFICATION OF IVORY BOOK COVERS<br />

from illuminated manuscripts, though declined<br />

in popularity by <strong>the</strong> time <strong>the</strong>se books were made.<br />

Cutting and veneering techniques were much<br />

<strong>the</strong> same, as well as consequent risks of deterioration.<br />

Similarities in history of ivory use, ivory processing,<br />

and risks of deterioration led to a comparison of<br />

<strong>conservation</strong> techniques. Though <strong>the</strong> book covers<br />

are in poor condition, it is due to <strong>the</strong> inherent vice<br />

of <strong>the</strong> ivory book structure. Thus, <strong>conservation</strong><br />

treatment may not yield lasting effects, so administering<br />

preventive <strong>conservation</strong> practices in order<br />

to prevent fur<strong>the</strong>r damage would be a more<br />

appropriate approach.<br />

Through research on <strong>the</strong> history of ivory use in<br />

book covers, it is evident that <strong>the</strong>re has been a<br />

long tradition which may have ended around <strong>the</strong><br />

time of <strong>the</strong>se three examples. They are thus in a<br />

stable enough condition to display <strong>the</strong> delicate<br />

and beautiful craftsmanship of ivory in <strong>the</strong> unique<br />

form of book covers. Fur<strong>the</strong>rmore, this comparison<br />

has revealed <strong>the</strong> impact that <strong>the</strong> growing knowledge<br />

of portrait miniatures in Canada is beginning<br />

to have on o<strong>the</strong>r areas of <strong>conservation</strong>.<br />

Acknowledgements<br />

The author would like to thank Library and Archives<br />

Canada as well as <strong>the</strong> following people for <strong>the</strong>ir<br />

invaluable assistance: Anne Maheux and Genevieve<br />

Samson at LAC for all <strong>the</strong>ir support; Scott Williams<br />

and Tom Stone at <strong>the</strong> Canadian Conservation Institute<br />

for examining and analyzing <strong>the</strong> ivory materials;<br />

Gayle McIntyre at Fleming College for her<br />

encouragement and feedback; Alan Derbyshire<br />

at <strong>the</strong> Victoria and Albert Museum for <strong>the</strong> use of<br />

his photographs; Maria Bedynski at LAC for sharing<br />

her expertise in portrait miniatures; and especially<br />

Lynn Curry at LAC for her inspiration and<br />

mentorship throughout this entire project.<br />

References<br />

[1] B. Burack, Ivory and its Uses, Charles E. Tuttle<br />

Company, Rutland, Vermont, USA, 1984<br />

[2] O. Krzyszkowska, Ivory and Related Materials: an<br />

Illustrated Guide, Institute of Classical Studies,<br />

London, 1990<br />

[3] I. M. Godfrey, “Ivory, Bone and Related Materials”,<br />

D. Gilroy and I. M. Godfrey (eds.) A Practical Guide<br />

to <strong>the</strong> Conservation and Care of Collections, Western<br />

Australian Museum, Perth, 1998, pp. 47-52<br />

[4] G. Matthaes, The Art Collector's Illustrated Handbook,<br />

Museo d'Arte e Scienza, Milan, 1997<br />

[5] J. Thornton, The Structure of Ivory and Ivory<br />

Substitutes, A.I.C. Preprints of Ninth Annual<br />

Meeting, Philadelphia, 1981, pp. 173-181<br />

[6] S. Williams, “The Diphenylamine Spot Test for Cellulose<br />

Nitrate in Museum Objects”, CCI Notes 17/2,<br />

Canadian Conservation Institute, Ottawa, 1994,<br />

URL (accessed October 2009)<br />

[7] S. Williams, CCI 120102: Near Infrared Spectroscopic<br />

Analysis of Ivory Book Covers, Canadian Conservation<br />

Institute, Ottawa, 2009, unpublished report<br />

[8] E. O. Espinoza, and M.-J. Mann, Identification Guide<br />

for Ivory and Ivory Substitutes, Washington D.C.,<br />

World Wildlife Fund and The Conservation Foundation,<br />

1991, URL (accessed September 2009)<br />

[9] C.L. Connor, The Color of Ivory: Polychromy on<br />

Byzantine Ivories, Princeton University Press,<br />

New Jersey, 1997<br />

[10] R.H. Randall Jr., Masterpieces of Ivory from <strong>the</strong><br />

Walters Art Gallery, Hudson Hills Press in association<br />

with <strong>the</strong> Walters Art Gallery, Baltimore, 1985<br />

[11] "Watercolour on Ivory", Victoria and Albert<br />

Museum, URL (accessed November 2009)<br />

[12] C. Aiken, “Literature that Addresses <strong>the</strong> Characterization<br />

and <strong>the</strong> Conservation of Portrait Miniatures”,<br />

Reviews in Conservation 1, 2000, pp. 3-9<br />

[13] J. Murrell, "Portrait Miniatures on Ivory: Problems<br />

of Technique and Style", Traitement des supports.<br />

e-<strong>conservation</strong><br />

37


JOSIE WORNOFF<br />

Travaux interdisciplinaires: journées sur la <strong>conservation</strong>,<br />

restauration des biens culturels, 1989,<br />

pp. <strong>16</strong>9-176<br />

[14] “Care of Ivory, Bone, Horn and Antler”, CCI Notes<br />

6/1, Canadian Conservation Institute, Ottawa,<br />

1988, URL (acessed September 2009)<br />

[15] C. Holtzapffel and J. C. Thompson, Working Horn,<br />

Ivory & Tortoiseshell, Portland, The Caber Press,<br />

2000<br />

[<strong>16</strong>] C. Aiken, "Ivory and <strong>the</strong> Art of Miniature Painting",<br />

Looking for Eulabee Dix: The Illustrated Biography<br />

of an American Miniaturist, National Museum of<br />

Women in <strong>the</strong> Arts, Washington, 1997, pp. 285-293<br />

[17] J.H. Pratt, “Improvement in Ivory Covered Books”,<br />

U.S. Patent No. 42,507 of April 26, 1864, United<br />

States Patent Office, New York, 1864<br />

[18] E. Cristoferi and C. Fiori, "Polishing Treatments<br />

on Ivory Materials in <strong>the</strong> National Museum Ravenna",<br />

Studies in Conservation 37, 1992, pp. 259<br />

[19] P.E. Guldbeck and A. B. MacLeish, Care of Antiques<br />

and Historical Collections, Rowman Altamira, 1996<br />

[20] K. Eirk, and W. Wiebold, Objects of Affection: The<br />

Conservation of Portrait Miniatures, National<br />

Museum of American Art, unpublished report<br />

[21] M.T. Simpson and M. Huntley (eds.), "Paintings:<br />

Miniatures", So<strong>the</strong>by’s Caring for Antiques: a guide<br />

to handling, cleaning, display and restoration,<br />

Markham, Canada Octopus Publishing Group Canada,<br />

1992, pp. 110-13<br />

[22] A. Derbyshire, “Restoration of miniatures on ivory.<br />

Sauvegarde et <strong>conservation</strong> des photographies,<br />

dessins, imprimés et manuscrits”, Actes des journées<br />

internationales d études de l’ARSAG, Paris, 30 sept.<br />

- 4 <strong>oct</strong>. 1991 (Paris, ARSAG, 1991) pp.147-151<br />

[23] C. Aiken and M. Bedynski, LAC Portrait Miniature<br />

Project Condition Reports, Ottawa, Library and<br />

Archives Canada, 2007, unpublished report<br />

[24] A. Derbyshire, N. Frayling and C. Rönnerstam,<br />

“Developments in <strong>the</strong> Field of Portrait Miniature<br />

Conservation”, Restauratorenblätter 21, 2000,<br />

pp. 53-59<br />

[25] M. Trojan-Bedynski and G. Gignac, “Portrait Miniatures:<br />

History, Materials, Techniques and Conservation”,<br />

30 th Canadian Association for Conservation<br />

Annual Conference, Quebec City, May 26-30,<br />

2004, Library and Archives Canada, 2004<br />

[26] A. Derbyshire, “The Use of Gore-tex in <strong>the</strong> Flattening<br />

of Miniatures on Ivory”, Paper Conservation<br />

News 63, 1992<br />

[27] C. Snow and T. Weisser, “The Examination and Treatment<br />

of Ivory and Related Materials”, Adhesives and<br />

Consolidants, The International Institute for Conservation<br />

of Historic and Artistic Works, London, 1984<br />

[28] F. Minney, "The Conservation and Reconstruction<br />

of a Late Bronze Age Ivory Inlaid Box from Palestine",<br />

The Conservator, vol. 15, 1991, pp. 3-7<br />

[29] Victoria and Albert Museum, “The Care of Ivory”,<br />

Technical Notes on <strong>the</strong> Care of Art Objects, no. 6,<br />

Victoria and Albert Museum, London, 1971<br />

JOSIE WORNOFF<br />

Paper Conservator<br />

Contact: josie.wornoff@utoronto.ca<br />

Josie Wornoff is an emerging paper conservator<br />

from Keene, Ontario, Canada. She began her postsecondary<br />

education with an Honours Bachelor<br />

of Arts at University of Toronto, majoring in Art<br />

History and English. During this time she held<br />

many volunteer and paid positions at various cultural<br />

institutions across Ontario, and spent two<br />

summers abroad studying art history in Italy and<br />

Mexico. Josie <strong>the</strong>n completed <strong>the</strong> Collections Conservation<br />

and Management program at Sir Sandford<br />

Fleming College. This concluded with a four<br />

month internship at Library and Archives Canada<br />

Preservation Centre, specializing in <strong>the</strong> <strong>conservation</strong><br />

of books and art on paper. Josie recently<br />

completed a project conserving a large collection<br />

of fire damaged art and artifacts for a private <strong>conservation</strong><br />

business in Florida. Currently, she is<br />

preserving books through digitization initiatives<br />

at Internet Archive Canada in Toronto.<br />

38 e-<strong>conservation</strong>


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

An Assessment of Enzyme Activity, Fungicides<br />

and Some Mummification Materials<br />

for <strong>the</strong> Inhibition of Microbial Deterioration<br />

by Abdelrazek Elnaggar, Ahmed Sahab,<br />

Siham Ismail, Gamal Mahgoub and<br />

Mohammed Abdelhady<br />

Fungal and bacterial strains were isolated from some Egyptian mummies (from <strong>the</strong> Ismailia<br />

Museum, Ismailiaa, Egypt; <strong>the</strong> El-Dokki Agriculture Museum in Cairo, Egypt and human<br />

mummies in storage at <strong>the</strong> Ehnasia Museum in Beni-Sweif, Egypt). The biological samples<br />

were taken from indoor air of <strong>the</strong> mummy chamber as well as from <strong>the</strong> linen bandages and<br />

some deteriorated mummies from museum storage. Seven species of fungi were isolated and<br />

identified as Alternaria tenuis (9.5%), Aspergillus humicola (23.8%), Aspergillus niger<br />

(23.8%), Chaetomella horrida (9.5%), Chaetomium globosum (14.28%), Hormodendrum<br />

viride (14.28%) and Penicillium corylophilum (4.9%). It is obvious from <strong>the</strong> morphological<br />

properties and biochemical activity of <strong>the</strong> microorganisms that <strong>the</strong>y were able to decompose<br />

proteins, cellulose, fats and starch, <strong>the</strong> fundamental contents of a mummy's body. The most<br />

prominent bacteria isolated were Halococcus morrhuae (30.76%), Streptococcus pyogenes<br />

(23.07%), Micrococcus Kristinae (15.38%), Micrococcus cinereus (15.38%) and Halobacterium<br />

pharaonis (13.38).<br />

Results show that A. niger, A. humicola, H. viride, and P. corylophilum were very sensitive<br />

to <strong>the</strong> mummification material of natron salt. The growth of P. corylophilum was completely<br />

inhibited at all concentrations of benlate and thymol while A. niger and H. viride were<br />

completely inhibited at all thymol concentrations and at 100 ppm of benlate fungicide. The<br />

growth of H. viride was completely inhibited at 5 % of cedar oil.<br />

The fungal isolates of A. niger, H. viride, and P. corylophilum were found to produce various<br />

amounts of extracellular enzymes (Avicelase, CMCase and cellobiase).These enzymes play an<br />

important role in deteriorating linen bandages as well as <strong>the</strong> mummy’s body.


ABDELRAZEK ELNAGGAR et al.<br />

Research Aims<br />

Figure 1. A human mummy at Ehnasia Museum, Beni-Sweif,<br />

Egypt.<br />

Figure 2. Isolation of biological samples from a mummy at<br />

Ehnasia Museum (Beni-Sweif, Egypt).<br />

The objectives of <strong>the</strong> present investigation are to<br />

study <strong>the</strong> fungal colonization and exoenzymatic<br />

activities of some deteriorated Egyptian mummies,<br />

and <strong>the</strong> effect of mummification materials on <strong>the</strong><br />

fungal growth to determine <strong>the</strong> efficiency of <strong>the</strong>se<br />

materials in <strong>the</strong> mummification process. Fur<strong>the</strong>rmore,<br />

ano<strong>the</strong>r important aim is to study <strong>the</strong> effect<br />

of some fungicides in preservation of mummies<br />

from fungal attack.<br />

Introduction<br />

Biodeterioration is considered a great factor in <strong>the</strong><br />

decomposition of <strong>the</strong> Egyptian mummies, because<br />

fungi and bacteria grow and feed with many of<br />

<strong>the</strong>ir constituent products, such as protein, fats,<br />

starch and cellulose, which represent a stable substrate<br />

to microbial growth. There are a number of<br />

abiotic and biotic factors such as pollution, light,<br />

humidity, temperature, microorganisms, insects,<br />

etc., that have deteriorating effects on museum<br />

materials [1]. Among <strong>the</strong>se, biological agents<br />

such as actinomycetes, fungi, bacteria etc., may<br />

cause massive damage to museum objects [2].<br />

Studies on indoor aeromycoflora have attracted<br />

<strong>the</strong> attention of several aerobiologists [2-5].<br />

Martinez et al. [6] isolated a total of 469 fungal<br />

colonies from 12 mummies that presented deterioration<br />

attributed to colonizing fungi. Among<br />

<strong>the</strong> isolated fungi Penicillium, Cladosporium and<br />

Aspergillus were found. Most of <strong>the</strong>se fungi have<br />

<strong>the</strong> ability to produce various enzymes (cellulases,<br />

amylases, proteases, keratinases, etc.). Cellulase<br />

enzymes degrade cellulose found in linen bandages<br />

to double sugars and endoglaconases enzymes<br />

cut <strong>the</strong> cellulose chain in a random fashion<br />

whereas, exogluconases enzymes successively<br />

remove single cellobiose or glucose units from<br />

<strong>the</strong> non-reducing end of <strong>the</strong> cellulose chain [7,<br />

8]. Many fungi are able to cause zoonotic superficial<br />

infections as a consequence of invading<br />

keratinize tissues of skin, hair, and nails [9, 10].<br />

Materials and methods<br />

Samples<br />

Biological samples were taken from a linen-wrapped<br />

mummy, from <strong>the</strong> air of mummy chambers and<br />

from deteriorated Egyptian mummies preserved<br />

in museum storage as follows: human mummy<br />

no. 2520 and 2519 from <strong>the</strong> Ismailia Museum (Ismailiaa,<br />

Egypt); animal mummies No. 35 and 93<br />

from <strong>the</strong> El-Dokki Agriculture Museum (Cairo, Egypt)<br />

and human mummies in storage at Ehnasia Museum<br />

(Beni-Sweif, Egypt, see figures 1,2). Sampling of<br />

40 e-<strong>conservation</strong>


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

air spora surrounding <strong>the</strong> above mummies was<br />

done using <strong>the</strong> plate exposure method [11].<br />

Isolation and identification of fungal strains<br />

Swaps from linen bandages wrapped mummies<br />

were transferred aseptically to potato dextrose<br />

agar plates [12] which were used for <strong>the</strong> cultivation<br />

of bacteria and moulds. The Petri dishes were<br />

incubated at 28 ± 2 °C for 7 days for fungi and 3<br />

days for bacterial counts. Fungal isolates were<br />

later microscopically analyzed and identified [13-<br />

15]. The scheme of Buchanan and Gibon [<strong>16</strong>] was<br />

employed in <strong>the</strong> identification of bacterial isolates.<br />

The frequency occurrence of each genus<br />

was expressed as <strong>the</strong> percentage of samples containing<br />

a given organism.<br />

Effect of some materials of mummification<br />

on fungal growth<br />

Each of <strong>the</strong> following mummification materials -<br />

natron, myrrh, juniperus, Cinnamomium camphora,<br />

Arabic gum, cassia, mastic resin, and beeswax -<br />

was separately examined for its effect on <strong>the</strong> visual<br />

growth of some selected fungi isolated from <strong>the</strong><br />

mummies using PDA plates. 1 ml of spore suspension<br />

(approximately 106/ ml) of 7 days old culture<br />

was placed in a Petri dish and poured by PDA medium.<br />

After solidification 0.2 g of <strong>the</strong> mummification<br />

material was put in <strong>the</strong> centre of <strong>the</strong> dish<br />

plate (1 cm diameter) and was fumigated by UV<br />

light. Dishes were incubated at 28 ± 2°C for 7 days.<br />

The developed colonies of various fungal growths<br />

were visually determined using <strong>the</strong> following<br />

scale: + (10% growth), ++ (50% growth), +++<br />

(75% growth) and ++++ (100 % growth).<br />

Effect of some fungicides on <strong>the</strong> linear growth<br />

of fungi<br />

Three kinds of fungicides recommended for use in<br />

archaeological field were tested in this experiment<br />

at different concentrations in order to ascertain<br />

<strong>the</strong>ir effect on <strong>the</strong> growth of fungi and <strong>the</strong>ir inhabitation<br />

effect. Table 1 shows <strong>the</strong> fungicides,<br />

<strong>the</strong>ir chemical name and composition, and <strong>the</strong> concentrations<br />

used based on <strong>the</strong> active ingredient.<br />

Table 1. Characteristics of <strong>the</strong> fungicides used.<br />

Fungicide Chemical name Chemical<br />

Thymol<br />

Benlate<br />

Cedar oil<br />

Thyme camphor<br />

Benomyl<br />

Cedar camphor<br />

composition<br />

Isopropylmetacresol<br />

(CH 3 ) 2 CHC 6 H 3<br />

(CH 3 ) OH<br />

Active ingredients<br />

(%)<br />

100<br />

Methyl-1- ( Bytyl<br />

carbamyl) - 2-<br />

benzimidazole 50<br />

carbamate<br />

C 15 H 18 N 4 O 3<br />

Cedrol<br />

C 15 H 26 O 100<br />

Concentrations<br />

0<br />

25 ppm<br />

50 ppm<br />

100 ppm<br />

200 ppm<br />

6.25 ppm<br />

12.5 ppm<br />

50 ppm<br />

100 ppm<br />

0<br />

0.5 %<br />

1 %<br />

2.5 %<br />

5 %<br />

e-<strong>conservation</strong><br />

41


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

rence as follows: Chaetomium globosum and Hormodendrum<br />

viride (14.28%) and Alternaria tenuis<br />

and Chaetomella horrida (9.5%). There are many<br />

reports dealing with <strong>the</strong> microbial levels, such as<br />

Abdel-Kareem et al. [21], Cook and Rayner [22],<br />

Darwish and Sahab [23].<br />

Five bacterial species belonging to four genera<br />

were identified and classified as: Halococcus morrhuae<br />

(30.76%), Streptococcus pyogenes (23.07%),<br />

Micrococcus Kristinae, Micrococcus cinereus and<br />

Halobacterium pharaonis (15.38%).<br />

Effect of some mummification materials on<br />

visual fungal growth<br />

The data in Table 2 shows that <strong>the</strong> mummification<br />

materials have different ability to inhibit <strong>the</strong> mycelial<br />

growth of <strong>the</strong> tested fungal isolates. The<br />

five strains of A. niger, H. viride, P. corylophilum<br />

and A. humicola were very sensitive to natron salt<br />

and relatively sensitive to a Cinnnamomum camphora<br />

extract (figure 3). The natron salts had a<br />

large effect on <strong>the</strong> growth of <strong>the</strong> fungal isolates<br />

because it inhibited <strong>the</strong> fungal growth on a large<br />

area, as <strong>the</strong> NaCl present in natron salt is an historic<br />

preservation material. On <strong>the</strong> o<strong>the</strong>r hand,<br />

<strong>the</strong> same fungal isolates were less affected by<br />

myrrh and beeswax extracts and <strong>the</strong> mummification<br />

materials of Juniperus, Arabic gum and cassia<br />

extracts were found to have no effect on <strong>the</strong> tested<br />

fungal growth.<br />

Enzymatic activity<br />

Enzyme activity of cellulase production in fungal<br />

strains was measured with different substrates<br />

Figure 3. From left to right: Effect of myrrh on <strong>the</strong> growth of Aspergillus humicola, effect of cinnamomium camphora on <strong>the</strong><br />

growth of Aspergillus humicola, and effect of cinnamomium camphora on <strong>the</strong> growth of Aspergillus niger.<br />

Table 2. Effect of some mummification materials on visual fungal growth of some fungal isolates after 15 days.<br />

Fungal species<br />

Aspergillus niger (strain no.)<br />

H. viride P. corylophilum A. humicola<br />

Strain no. 1 2 3 4 5<br />

Natron + + + ++ + + ++ +<br />

Myrrh +++ ++ ++ +++ +++ ++ ++ ++<br />

Juniperus ++++ ++++ ++++ ++++ ++++ ++++ ++++ ++++<br />

Cinnamomum camphora +++ +++ +++ +++ +++ ++++ ++ ++<br />

Arabic gum ++++ ++++ ++++ ++++ ++++ ++++ ++++ ++++<br />

Cassia ++++ ++++ ++++ ++++ ++++ ++++ ++++ ++++<br />

Mistic resin ++++ ++++ ++++ ++++ ++++ +++ ++++ ++++<br />

Beeswax +++ +++ +++ +++ +++ ++ ++ +++<br />

control ++++ ++++ ++++ ++++ ++++ ++++ ++++ ++++<br />

Legend: + (10% fungal growth), ++ (50% fungal growth), +++ (75% fungal growth), ++++ (100 % fungal growth).<br />

e-<strong>conservation</strong><br />

43


ABDELRAZEK ELNAGGAR et al.<br />

(cellulose, protein, fats, and starch) to know <strong>the</strong><br />

ability of <strong>the</strong>se fungi to produce <strong>the</strong>se enzymes<br />

that react with <strong>the</strong> mummy’s skin and wrappings<br />

causing its decomposition. The results shown in<br />

Tables 3-5 reveal that all <strong>the</strong> tested fungi produced<br />

various amounts of extracellular enzymes (Avicelase,<br />

CMCase and cellobiase). The value of enzyme<br />

production depended on <strong>the</strong> fungal species and<br />

age of <strong>the</strong> culture. The ability of <strong>the</strong>se fungi to<br />

decompose casein, cellulose, oil and starch has<br />

also been confirmed by o<strong>the</strong>r researchers.<br />

a) Avicelase enzyme<br />

The tested fungi showed feeble Avicelase activity<br />

ranging from 0.041 U/ml to 0.115 U/ml for A. niger,<br />

from 0.001 to 0.143 U/ml for H. viride and<br />

from 0.009 to 0.399 U/ml for P. corylophilum after<br />

5 and 20 days respectively (Table 3). The highest<br />

activity of Avicelase was recorded for cellulose<br />

following casein substrates.<br />

b) CMCase enzyme<br />

Table 4 showed that all <strong>the</strong> tested fungi produced<br />

different values of extracellular CMCase ranging<br />

from 0.103 to 0.643 U/ml for A. niger, from 0.013<br />

to 2.050 U/ml for H. viride and from 0.010 to 1.136<br />

U/ml for P. corylophilum. The highest activity of<br />

MCase was recorded for cellulose and casein substrates.<br />

Many authors [24, 25, 26, and 27] reported<br />

that all tested fungi had <strong>the</strong> ability to decompose<br />

cellulosic materials and produce cellulase<br />

enzymes.<br />

Table 3. Effect of some substrates on Avicelase activity of some fungal strains isolated from mummies and incubated for 5, 7 and<br />

20 days at 28± 2°C.<br />

Fungal strain A. niger H. viride P. corylophilum<br />

Incubation<br />

period/day<br />

5 7 20 5 7 20 5 7 20<br />

Casein 0.027 0.114 0.115 0.093 0.05 0.105 0.027 0.114 0.046<br />

Cellulose 0.021 nd 0.08 0.109 nd 0.143 0.1197 nd 0.399<br />

Oil 0.014 0.06 nd 0.0147 0.018 0.022 0.009 0.029 0.057<br />

Starch 0.021 0.024 0.032 0.001 0.007 0.014 0.0143 0.056 0.013<br />

Nd: not determined<br />

Table 4: Effect of some substrates on CMCase activity of some fungal strains isolated from mummyies and incubated for 5, 7 and<br />

20 days at 28± 2°C.<br />

Fungal strain A. niger H. viride P. corylophilum<br />

Incubation<br />

period/day<br />

5 7 20 5 7 20 5 7 20<br />

Casein 0.311 0.321 0.643 0.643 0.571 0.06 0.122 0.322 0.099<br />

Cellulose 0.321 nd 1.210 0.205 nd 0.296 0.928 nd 1.136<br />

Oil 0.45 0.024 nd 0.09 0.013 0.013 0.01 0.028 nd<br />

Starch 0.103 0.123 0.139 0.043 0.43 0.69 0.013 0.095 0.114<br />

Nd: not determined<br />

44 e-<strong>conservation</strong>


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

Table 5: Effect of some substrates on cellobiase activity of some fungal strains isolated from mummies and incubated for 5, 7<br />

and 20 days at 28± 2°C.<br />

Fungal strain A. niger H. viride P. corylophilum<br />

Incubation<br />

period/day<br />

5 7 20 5 7 20 5 7 20<br />

Casein 4.69 5.556 5.69 0.279 0.393 3.703 0.228 0.831 5.74<br />

Cellulose 4.843 nd 6.389 0.293 nd 3.703 0.243 nd 1.179<br />

Oil 4.89 6.482 6.945 0.105 0.115 0.122 0.064 0.064 0.02<br />

Starch 7.861 5.556 5.463 0.125 0.209 0.293 1.389 2.778 4.877<br />

Nd: not determined<br />

c) Cellobiase enzyme<br />

Table 5 shows that <strong>the</strong> highest cellobiase activity<br />

(7.861 U/ml) was obtained from <strong>the</strong> culture filtrate<br />

of A. niger after 5 days on starch substrate<br />

and <strong>the</strong> lower level (4.690 U/ml) on casein. In<br />

H. viride culture filtrate <strong>the</strong> highest value (3.703<br />

U/ml) was shown on cellulose substrate and <strong>the</strong><br />

lowest level (0.105 U/ml) on oil substrate after<br />

5 days incubation period. High level of cellobiase<br />

activity (5.740 U/ml) was obtained in culture filtrate<br />

of P. corylophilum after 20 days on casein<br />

substrate and lower cellobiase (0.020 U/ml) was<br />

showed on oil after 20 days. The production of<br />

cellobiase from different fungi was reported by<br />

several authors [25, 28, 29, 30].<br />

Effect of some fungicides on <strong>the</strong> linear growth<br />

of some fungi<br />

Table 6 shows <strong>the</strong> effect of some fungicides as<br />

agar amendment on <strong>the</strong> mycelial linear growth<br />

(A. niger, H. viride and P. corylophilum). Data indicate<br />

that <strong>the</strong> antifungal activity of benlate, thymol<br />

and cedar oil against fungal growth increased<br />

with <strong>the</strong> growth in fungicide concentration. The<br />

linear growth of P. corylophilum was completely<br />

inhibited at all concentrations of benlate and<br />

thymol while <strong>the</strong> growth of A. niger and H. viride<br />

was also completely inhibited at all concentrations<br />

of thymol and benlate at 100 ppm. The growth of<br />

H. viride was completely inhibited at 5% of cedar<br />

Table 6. Effect of some fungicides on <strong>the</strong> linear fungal growth of some fungi isolated from mummies.<br />

Fungi Benlate fungicide concentration (ppm) Mean<br />

0 6.25 12.5 50.0 100.0<br />

Aspergillus niger<br />

Hormodendrum viride<br />

Penicillium corylophilum<br />

100.0 70.0 33.3 22.2 0.0<br />

100.0 80.0 72.1 60.0 0.0<br />

100.0 0.0 0.0 0.0 0.0<br />

Thymol concentration (ppm)<br />

0 25 50 100 200<br />

45.1<br />

62.4<br />

20.0<br />

Aspergillus niger<br />

Hormodendrum viride<br />

Penicillium corylophilum<br />

100.0 75.5 63.6 42.6 0.0 56.3<br />

100.0 0.0 0.0 0.0 0.0 20.0<br />

100.0 0.0 0.0 0.0 0.0 20.0<br />

e-<strong>conservation</strong><br />

45


ABDELRAZEK ELNAGGAR et al.<br />

Fungi Cedar oil concentration (%) Mean<br />

0 0.5 1.0 2.5 5.0<br />

Aspergillus niger<br />

Hormodendrum viride<br />

Penicillium corylophilum<br />

100.0 100.0 75.5 70.8 60.0<br />

100.0 100.0 80.2 20.0 0.0<br />

100.0 85.6 76.8 65.9 65.0<br />

81.3<br />

60.0<br />

78.7<br />

oil. These results are in total agreement with those<br />

reported by o<strong>the</strong>r researches on several fungi [31].<br />

Cleaning procedures<br />

Removal of microbial stains and growths over <strong>the</strong><br />

mummies has been carried out using scalpels and<br />

soft brushes accompanied with an extraction system,<br />

to reduce <strong>the</strong> spore's contamination in <strong>the</strong><br />

working area (figure 4). Cleaning started from <strong>the</strong><br />

middle to <strong>the</strong> edges to easily collect <strong>the</strong> fungal<br />

growths and dirt particles without <strong>the</strong> spread of<br />

<strong>the</strong> microbial contamination (figure 5). Isopropyl<br />

alcohol has been used to sterilize <strong>the</strong> cleaning<br />

equipment and <strong>the</strong> surrounding environments<br />

during and after cleaning (figures 6-7). White free<br />

acid papers have been place below <strong>the</strong> mummy<br />

to better collect <strong>the</strong> fungal conidia. Benlate fungicide<br />

(200 ppm) has been applied on <strong>the</strong> mummy's<br />

wrapping using a sprayer. After cleaning, mummies<br />

were covered by polyethylene to protect <strong>the</strong>m<br />

from fur<strong>the</strong>r contamination. For health and safety<br />

issues, <strong>the</strong> conservator must wear a mask, coat,<br />

goggles and gloves during cleaning to avoid inhalation<br />

of <strong>the</strong> microbial contaminants (figure 8).<br />

Figure 4. Mummy's head wrappings during cleaning.<br />

Figure 5. Mummy's wrappings after cleaning.<br />

Conclusion<br />

After isolation of <strong>the</strong> microbial species from Egyptian<br />

mummies, experimental studies confirmed<br />

<strong>the</strong> efficiency of some of mummification materials<br />

on <strong>the</strong> inhibition of fungal growth, indicating<br />

that mummification materials may also function<br />

as biocides. The study indicates <strong>the</strong> ability of <strong>the</strong><br />

Figure 6. Sterilization of <strong>the</strong> surrounding air during cleaning.<br />

46 e-<strong>conservation</strong>


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

Figure 7. Collecting and removal of dirt particles and fungal<br />

growths from a mummy.<br />

Figure 8. The necessary tools for conservator' health and<br />

safety (masks, gloves, goggles).<br />

isolated fungal strains from <strong>the</strong> Egyptian mummies<br />

to produce various amounts of extracellular enzymes<br />

(Avicelase, CMCase and cellobiase) which<br />

may lead to <strong>the</strong> decomposition of <strong>the</strong> mummy<br />

materials. Benlate, thymol and cedar oil show an<br />

ability to inhibit fungal growth. The authors would<br />

like to recommend creating better preventive <strong>conservation</strong><br />

procedures in order to preserve <strong>the</strong> mummies<br />

from future damage.<br />

References<br />

[1] A. E. David, “Conservation of mummified Egyptian<br />

Remains”, in A. R. David (ed.), in Science<br />

in Egyptology: proceedings of <strong>the</strong> Science in<br />

Egyptology Symposia, Manchester University<br />

Press, Manchester, 1986.<br />

[2] A. Arya, A. R. Shah, and S. Sadasivan, “Indoor<br />

aeromycoflora of Baroda museum and deterioration<br />

of Egyptian mummy”, Current Science<br />

81(7), 2001, URL<br />

[3] P.H. Gregory, Microbiology of <strong>the</strong> Atmosphere,<br />

Leonard Hill Books, Aylesbury, England, 1973,<br />

pp. 377<br />

[4] A. F. Sahab, F. Tawfic, S. Sahaba, and S. Mous-<br />

tafa, “Indoor fungal airospora and microorganisms<br />

communities associated with old manuscripts<br />

of GEBO of Egypt”, Journal of Agricultural<br />

Sciences 28(8), Mansoura University,<br />

2003, pp. 6055- 6063<br />

[5] K. Zielinska-Jankiewicz, A. Kozajda, M. Piotrowska,<br />

and I. Szadkowska-Stanczyk, “Microbiological<br />

contamination in moulds in work<br />

environment in libraries and archive storage<br />

facilities”, Annals of Agricultural and Environmental<br />

Medicine 15, 2008, pp. 71-78<br />

[6] R. López-Martínez, F. Hernández-Hernández,<br />

B.E. Millán-Chiu, P. Manzano-Gayosso, and L.<br />

J. Méndez-Tovar, “Effectiveness of imazalil to<br />

control <strong>the</strong> effect of fungal deterioration on<br />

mummies at <strong>the</strong> Mexico City Museum ‘El Carmen’”<br />

(article in Spanish), Revista Iberoamericana<br />

de Micología 24, 2007, pp. 283-288<br />

[7] R. A. Zabel, and J. J. Morrell, Wood microbiology:<br />

decay and its prevention, Academic<br />

Press, San Diego, 1992<br />

[8] T. Reinikainen, K. Henriksson, M. Siika-aho,<br />

O. Teleman and K. Poutanen, “Low-level endoglucanase<br />

contamination in a Trichoderma<br />

e-<strong>conservation</strong><br />

47


MICROBIAL STUDY OF EGYPTIAN MUMMIES<br />

[25] K.H. Domsch, W. Gams, and T.H. Anderson<br />

(eds), Compendium of Soil Fungi, Vol. 1, IHW-<br />

Verlag, Eching, Germany, 1993<br />

ABDELRAZEK ELNAGGAR<br />

Conservation-educator<br />

Contact: aaa02@fayoum.edu.eg<br />

[26] S. A. Ismail, Biochemical studies on Microbial<br />

β-Galactosidases, PhD Thesis, Chemistry<br />

Deptartment, Faculty of Science, Cairo University<br />

(Egypt), 1994<br />

[27] S.A. Ismail, A. F. Sahab, and S.S. Darwish,<br />

“Effect of some cultural conditions, pesticides<br />

and consolidators on growth and enzme activity<br />

of Trichoderma viride”, Modelling, Measurement<br />

and Control – C: Chemistry, Geology, Environment<br />

and Bioengineering 66 (5-6), 2005<br />

[28] C. Marinescu, and V. I. Popa, "On <strong>the</strong> biosyn<strong>the</strong>sis<br />

and characterization of cellulosic enzymes.<br />

II. Cellulase production enhancement<br />

in different biosyn<strong>the</strong>sis conditions”, Cellulose<br />

Chemistry and Technology 34, 2000, pp. 35-49<br />

[29] M. Rocha, N. Cordeiro, A.C.F. Cunha Queda,<br />

and R. Capela, “Microbiological and chemical<br />

characterization during composting of cattle<br />

manure and forestry wastes – a case study<br />

in Madeira Island”, in F. C. Jr. Michel, R. F.<br />

Rynk, and H. A. J. Hoitink (eds.), Proceedings<br />

of <strong>the</strong> 2002 International Symposium “Com<br />

posting and Compost Utilization”, The JG Press<br />

Inc., Emmaus, pp. 156-170<br />

[30] S. Y. Sahaba, Physiological studies on microorganisms<br />

isolated from deteriorated from old<br />

manscripts, Master Thesis, Faculty of Agriculture,<br />

Ain Shams University (Egypt), 1988<br />

[31] A. H. A. Ellil, and E. F. Sharaf, “Growth, Morphological<br />

Alterations and Adaptation of<br />

Some Plant Pathogenic Fungi to Benlate and<br />

Zineb. A New Look”, Journal of Biological Sciences<br />

3(3), 2003, pp. 271-281<br />

Abdelrazek Elnaggar is a conservator of organic<br />

objects, currently Assistant Lecturer at <strong>the</strong> Conservation<br />

Department of <strong>the</strong> Faculty of Archaeology<br />

at Fayoum University, Egypt. He got a Bachelor’s<br />

degree (2000) in Conservation and Restoration<br />

of Monuments and Works of Art from <strong>the</strong> Cairo<br />

University and a Master’s degree (2006) in Conservation<br />

of Egyptian mummies from Cairo University.<br />

He had a scholarship (2007/2008) in laser cleaning<br />

of ancient Egyptian Lea<strong>the</strong>r at IESL-FORTH in Greece<br />

and received a postgraduate diploma in comparative<br />

studied on cleaning techniques in relation to<br />

Laser cleaning <strong>conservation</strong> (2008/2009 UK).<br />

He has an ongoing PhD <strong>the</strong>sis focusing on <strong>the</strong><br />

laser applications to <strong>conservation</strong> of Egyptian<br />

monuments, including collaborative projects in<br />

UK with Liverpool University, Natural History<br />

Museum, Petrie museum, Imperial College, and<br />

UCL, in Italy with Politecnico di Milano, and <strong>the</strong><br />

Supreme Council of Antiquities (Egypt).<br />

AHMED SAHAB<br />

Department of Plant Path., National Research<br />

Centre, Dokki, Cairo<br />

SIHAM ISMAIL<br />

Department of Chemistry of Natural Microbial<br />

Products, National Research Centre, Dokki<br />

GAMAL MAHGOUB<br />

Conservation Department, Faculty of Archaeology,<br />

Fayoum University, Alfayoum, Egypt<br />

MOHAMMED ABDELHADY<br />

Conservation Department, Faculty of Archaeology,<br />

Cairo University, Giza, Egypt<br />

e-<strong>conservation</strong><br />

49


case study<br />

STUDY OF THE PAINTING VIRGIN MARY<br />

AND CHILD WITH THE INFANT<br />

ST. JOHN THE BAPTIST<br />

The Hidden Flora of Leonardo da Vinci’s<br />

Painting Workshop<br />

By Miklós Szentkirályi<br />

Article translated by Barbara and Stevin John Davidson and<br />

originally published in <strong>the</strong> Proceedings of <strong>the</strong> 8 th International<br />

Seminar on Restoration, that took place in September 24-26,<br />

2008 in Handlová, The Slovak Republic, organized by <strong>the</strong><br />

Chamber of Restorers.


THE HIDDEN FLORA OF LEONARDO DA VINCI’S PAINTING WORKSHOP<br />

Restoration of any damaged artwork should remind us of a flower garden grown with plenty of love.<br />

In both cases it is crucial to consider what has already blossomed and 'what has still to live'.<br />

This idea guided me through <strong>the</strong> process of restoration of this unusually damaged panel painting.<br />

Virgin Mary and Child with <strong>the</strong> Infant St. John <strong>the</strong> Baptist. Painting before <strong>conservation</strong>-restoration.<br />

e-<strong>conservation</strong> 51


MIKLÓS SZENTKIRÁLYI<br />

The painting in study, representing <strong>the</strong> Virgin Mary<br />

with Child Jesus and young St. John <strong>the</strong> Baptist<br />

from <strong>the</strong> collection of Szépművészeti Museum in<br />

Budapest, was never exhibited due to its advanced<br />

deterioration state and only a few people have<br />

undertaken its study. The support, made of a thin<br />

poplar panel, had caused countless vertical cracks<br />

to appear on <strong>the</strong> surface that interfered with <strong>the</strong><br />

integrity of <strong>the</strong> painting’s composition. The painting<br />

was covered with several layers of darkened<br />

varnish resulting in <strong>the</strong> alteration of <strong>the</strong> colour<br />

scheme that was only partially perceivable and<br />

<strong>the</strong> image could hardly be recognised. On a few<br />

areas <strong>the</strong> polychromy detached and <strong>the</strong> colour<br />

layer was flaking. Extensive over paintings were<br />

<strong>the</strong> characteristic sign of <strong>the</strong> advanced stage of<br />

damage of <strong>the</strong> painting’s surface. Large lacunas<br />

in <strong>the</strong> area of <strong>the</strong> sky, grazes and detachments<br />

on <strong>the</strong> face and neck of Virgin Mary and loss of<br />

colour on her cloths were critical. These damages<br />

were symptoms of a work of art which was not<br />

cared for and left to decay.<br />

Aspect of <strong>the</strong> painting after cleaning.<br />

The poor state of <strong>conservation</strong> of Mary's portrait.<br />

Aspect after <strong>conservation</strong>-restoration treatment.<br />

52 e-<strong>conservation</strong>


THE HIDDEN FLORA OF LEONARDO DA VINCI’S PAINTING WORKSHOP<br />

After <strong>the</strong> preliminary tests, <strong>the</strong> outstanding painting<br />

technique of this artwork became visible, with<br />

its rich colour scheme and true depiction of <strong>the</strong><br />

background landscape. But unexpected mistakes<br />

and insufficiencies were also revealed.<br />

Above: Network of fine cracks on <strong>the</strong> surface of Child’s<br />

portrait (left). Aspect after retouching (right).<br />

Below: Detail of <strong>the</strong> rich background of <strong>the</strong> painting.<br />

Based on <strong>the</strong> research done by <strong>the</strong> conservatorrestorers<br />

a proposal for <strong>the</strong> treatment of <strong>the</strong> painting<br />

was developed which was accepted by <strong>the</strong><br />

consultants.<br />

The extent of <strong>the</strong> cleaning and <strong>the</strong> complete uncovering<br />

of <strong>the</strong> original allowed a better understanding<br />

of <strong>the</strong> spiritual strength of Leonardo da<br />

Vinci (1452-1519) workshop’s creation. Observing<br />

this rediscovered artwork brings to mind a resemblance<br />

hard not to notice with both variations of<br />

<strong>the</strong> Madonna of <strong>the</strong> rocks, which can be found in<br />

<strong>the</strong> National Gallery, London and in <strong>the</strong> Louvre<br />

Museum, Paris, with <strong>the</strong>ir beautiful colour harmonies,<br />

mysterious play of lights and shades, rocks<br />

and flowers.<br />

The composition of <strong>the</strong> painting is closed with a<br />

half circle area in <strong>the</strong> upper part. The landscape<br />

contains a monolith rock towering into <strong>the</strong> sky,<br />

a beech forest, a grove and a water pothole. Virgin<br />

Mary is kneeling, raising her hands in a protective<br />

way over her Child and <strong>the</strong> young St. John <strong>the</strong><br />

Baptist, who are carelessly playing in <strong>the</strong> foreground<br />

decorated with rich flora and vegetation.<br />

e-<strong>conservation</strong> 53


MIKLÓS SZENTKIRÁLYI<br />

In background, behind <strong>the</strong> rock, <strong>the</strong>re is a river<br />

valley with a city disappearing in a bluish mist.<br />

Over <strong>the</strong> city <strong>the</strong>re is a scaffold with gallows. Fur<strong>the</strong>r<br />

in <strong>the</strong> back, bluish towers and hills, outlined<br />

according to <strong>the</strong> principles of air perspective, lose<br />

<strong>the</strong>mselves and blend with <strong>the</strong> clear blue sky.<br />

After <strong>the</strong> Madonna by Giovanni Antonio Boltraffio<br />

(1467-15<strong>16</strong>), <strong>the</strong> painting at <strong>the</strong> Museum of Fine<br />

Arts in Budapest is <strong>the</strong> closest to Leonardo’s creation.<br />

After analysing it in individual details, it<br />

became clear that it can not be <strong>the</strong> work of <strong>the</strong><br />

great master, although it is likely that he saw <strong>the</strong><br />

painting during its creation and perhaps even corrected<br />

it, since <strong>the</strong> basic idea of <strong>the</strong> composition<br />

belongs to him. In fact, a drawing from Leonardo’s<br />

sketchbook served as template for <strong>the</strong> creation<br />

of Mary’s figure [1], which could only be seen by<br />

an artist from Leonardo’s closest circle. Who this<br />

artist was is subject to future research, once <strong>the</strong><br />

painting’s known history requires more answers.<br />

Above right: Detail of <strong>the</strong> rich background of <strong>the</strong> painting.<br />

Below: Detail of Child Jesus and <strong>the</strong> young St. John <strong>the</strong><br />

Baptist playing in <strong>the</strong> rich decorated foreground.<br />

54 e-<strong>conservation</strong>


THE HIDDEN FLORA OF LEONARDO DA VINCI’S PAINTING WORKSHOP<br />

The only known fact is that count János Pálffy<br />

bought it in London in 1862. It was probably <strong>the</strong>n<br />

when <strong>the</strong> panel was parqueted. In 1912 <strong>the</strong> count<br />

offered it as a gift to <strong>the</strong> Szépművészeti Museum.<br />

Drawings from Leonardo's sketchbook served as a template<br />

for <strong>the</strong> creation of Mary’s figure.<br />

For a long time, <strong>the</strong> painting was considered to<br />

be <strong>the</strong> work of Leonardo’s pupil Gian Giacomo<br />

Caprotti da Oreno, known as Salai (1480-1524),<br />

although <strong>the</strong>re is no evidence for this assumption.<br />

Bernhard Berenson, who was <strong>the</strong> first recognised<br />

researcher of Italian fine art from <strong>the</strong><br />

14 th to <strong>16</strong> th century, considered (twice, in 1932<br />

and 1936) <strong>the</strong> painting to be <strong>the</strong> creation of one<br />

of Leonardo’s pupils whose work was also influenced<br />

by <strong>the</strong> Flemish art.<br />

Despite <strong>the</strong> fact that <strong>the</strong> painting was examined<br />

by specialists, we are still only uncovering analogies<br />

and stylistic analyses. The clarification of <strong>the</strong><br />

authorship will certainly be an important aspect in<br />

<strong>the</strong> study of <strong>the</strong> artwork and of <strong>the</strong> <strong>conservation</strong>restoration<br />

documentation done by <strong>the</strong> present<br />

author and his colleagues: conservator-restorer<br />

Ágnes Dicső, who has participated to <strong>the</strong> <strong>conservation</strong><br />

treatment and conservator-restorer Èva<br />

Galambos, who has performed <strong>the</strong> samples analysis<br />

of <strong>the</strong> painting.<br />

A number of people were also involved in <strong>the</strong> stylistic<br />

analysis of <strong>the</strong> painting and in <strong>the</strong> identification<br />

of <strong>the</strong> drawings and paintings from Leonardo’s<br />

workshop. Nadia Righi [2] has proved<br />

that <strong>the</strong> figure of Mary copies <strong>the</strong> shapes of <strong>the</strong><br />

drawing found on <strong>the</strong> bottom of a page from Leonardo’s<br />

sketchbook [1]. On <strong>the</strong> same page, as<br />

an independent drawing, is also pictured Child<br />

Jesus. This figure is similar with that of <strong>the</strong> Jesus<br />

from <strong>the</strong> painting, except his mirrored position.<br />

Ano<strong>the</strong>r similitude as a mirrored projection seams<br />

to be Mary’s profile to a Madonna (The Madonna<br />

Litta) from <strong>the</strong> Hermitage Museum in St. Petersburg.<br />

Fur<strong>the</strong>rmore, on <strong>the</strong> drawing template [3]<br />

of that painting an earlobe is recognizable behind<br />

<strong>the</strong> curls of her hair, which is similar to <strong>the</strong> one of<br />

our painting. It is also very likely that <strong>the</strong> concept<br />

of <strong>the</strong> composition of <strong>the</strong> young St. John <strong>the</strong><br />

Baptist, looking from behind Mary’s right side,<br />

e-<strong>conservation</strong> 55


MIKLÓS SZENTKIRÁLYI<br />

is derived from one of Leonardo’s templates, as<br />

well as <strong>the</strong> plants pictured in <strong>the</strong> front.<br />

Before cleaning, a stratigraphic analysis was performed<br />

in order to study <strong>the</strong> paint layer structure.<br />

Mary’s face and hair were well preserved and due<br />

to <strong>the</strong>ir similarity to those of <strong>the</strong> sketch we immediately<br />

observed <strong>the</strong> under drawing, made with<br />

brown colour. The preparatory under drawing<br />

can only be found under <strong>the</strong> composition of <strong>the</strong><br />

figures, and not under <strong>the</strong> background landscape.<br />

After <strong>the</strong> removal of <strong>the</strong> thick darkened varnish<br />

layer and of <strong>the</strong> over painting, all <strong>the</strong> degradations,<br />

grazes and lacunas became obvious. The<br />

damages and <strong>the</strong> missing parts were repaired at<br />

least three times in <strong>the</strong> past, especially at <strong>the</strong><br />

level of <strong>the</strong> figures. The details of <strong>the</strong> landscape<br />

were almost completely well preserved.<br />

The retouching of <strong>the</strong> lacunas was performed gradually<br />

and only in <strong>the</strong> necessary amount, except for<br />

Mary’s neck which required a more complex reconstruction<br />

due to <strong>the</strong> fact that <strong>the</strong> colour layer<br />

was only preserved in fragmentary traces but<br />

still allowing <strong>the</strong> aes<strong>the</strong>tical revitalisation of<br />

<strong>the</strong> painting. The fine craquelure network and<br />

<strong>the</strong> slightly scuffed areas were interpreted and<br />

accepted as signs of aging with time and <strong>the</strong>refore<br />

were preserved as much as possible. Only<br />

after restoration <strong>the</strong> unique aes<strong>the</strong>tical qualities<br />

of <strong>the</strong> preserved parts of <strong>the</strong> original painting<br />

could be fully appreciated and <strong>the</strong> differences between<br />

<strong>the</strong> painting technique of <strong>the</strong> background<br />

landscape and of <strong>the</strong> figures could be evaluated.<br />

In reality, our eye is attracted more to <strong>the</strong> richness<br />

of <strong>the</strong> landscape details. The view of <strong>the</strong> nor<strong>the</strong>rn<br />

Italian city in clear blue colours, with <strong>the</strong> houses<br />

blending in a bluish mist, <strong>the</strong> uniform conception<br />

of <strong>the</strong> water surfaces and of <strong>the</strong> rocks in <strong>the</strong> background<br />

prove <strong>the</strong> demanding approach of <strong>the</strong><br />

Above: Erythronium dens-canis (en., 'dog's tooth violet', it.,<br />

'dente di cane') in <strong>the</strong> painting (left) and <strong>the</strong> biology<br />

drawing of <strong>the</strong> flower (right).<br />

56 e-<strong>conservation</strong>


THE HIDDEN FLORA OF LEONARDO DA VINCI’S PAINTING WORKSHOP<br />

Dianthus carthusianorum.<br />

Pinguicula vulgaris, carnivorous plant.<br />

Aquilegia vulgaris L.<br />

painter. Our attention is also drawn to smaller details<br />

such as <strong>the</strong> stones that can be counted individually<br />

in <strong>the</strong> undermined bank. A few decades<br />

earlier, <strong>the</strong> Italian masters could only have admired<br />

<strong>the</strong>se motifs in <strong>the</strong> paintings of <strong>the</strong>ir Flemish contemporaries.<br />

The depiction of <strong>the</strong> plants in <strong>the</strong> foreground proves<br />

<strong>the</strong> knowledge of botany of <strong>the</strong> renaissance artists.<br />

The colours of <strong>the</strong> flowers petals are not only a<br />

simple decoration, on <strong>the</strong> contrary, similarly to<br />

<strong>the</strong> flowers found in Leonardo’s artworks, <strong>the</strong>y<br />

can be ordered into existing families. We can recognise<br />

Dianthus carthusianorum, favored flower<br />

of monastery gardens with its lance-shaped leaves,<br />

with two stamens between its bright two petals.<br />

Pictured in a more humble way is <strong>the</strong> Erythronium<br />

dens-canis next to it. In Italian, dente di cane<br />

is a protected plant named according to its bulb,<br />

similar to a dog’s tooth with smaller side bulbs<br />

placed deep into <strong>the</strong> ground, which in spring time<br />

is an embellishment of <strong>the</strong> hornbeam forests. To<br />

<strong>the</strong> right <strong>the</strong>re is a Pinguicula vulgaris, a carnivorous<br />

plant found in marshlands and peat bogs.<br />

On <strong>the</strong> left side of <strong>the</strong> painting is wonderfully<br />

painted Aquilegia vulgaris L. whose composition<br />

is almost identical to <strong>the</strong> same flower from Leonardo’s<br />

painting Leda.<br />

e-<strong>conservation</strong> 57


MIKLÓS SZENTKIRÁLYI<br />

Virgin Mary and Child with <strong>the</strong> Infant St. John <strong>the</strong> Baptist. Painting after restoration.<br />

58 e-<strong>conservation</strong>


THE HIDDEN FLORA OF LEONARDO DA VINCI’S PAINTING WORKSHOP<br />

Several similarities remind of <strong>the</strong> spirit of Leonardo’s<br />

workshop’s creation, strongly spiced up<br />

by a nor<strong>the</strong>rn Italian master. This fact became clear<br />

during <strong>the</strong> three years of restoration. The difference<br />

between <strong>the</strong> figures and <strong>the</strong> background<br />

composition is a strong sign of different creative<br />

approaches. While <strong>the</strong> painter’s grasp of <strong>the</strong> figures<br />

is generous, <strong>the</strong> painting technique being<br />

related to Leonardo’s understanding, <strong>the</strong> background<br />

landscape is carefully composed and a rich<br />

vegetation is portrayed. The exhaustive knowledge<br />

of <strong>the</strong> perspective rules, botany and <strong>the</strong><br />

naturalistic depiction of <strong>the</strong> landscape are signs<br />

of a master who had acquired <strong>the</strong> practical experience<br />

of painters from nor<strong>the</strong>rn countries before<br />

having contact with Leonardo’s workshop.<br />

The panel painting, restored thanks to <strong>the</strong> Adam<br />

Clark’s Foundation, was first introduced toge<strong>the</strong>r<br />

with <strong>the</strong> restoration documentation at a temporary<br />

exhibition in 2007. Since 2008 it is exhibited<br />

in a room toge<strong>the</strong>r with Raphael's "Esterhazy<br />

Madonna", as part of <strong>the</strong> permanent collection<br />

of Italian renaissance.<br />

Detail of Mary's portrait and <strong>the</strong> landscape after restoration.<br />

MIKLÓS SZENTKIRÁLYI<br />

Conservator-restorer<br />

Contact: miklos.szentkiralyi@szepmuveszeti.hu<br />

References<br />

[1] Leonardo da Vinci, “Studies for <strong>the</strong> Nativity<br />

(recto); Three Geometrical Diagrams and a<br />

Caricature of a Head (verso), 1480–85”, The<br />

Metropolitan Museum of Art, Rogers Fund,<br />

1917 (17.142.1), available at URL<br />

[2] Nadia Righi, “Opere d'arte lombarda nei<br />

musei italiani e stranieri: Szépmüveszéti<br />

Múzeum, Budapest; la collezione Pálffy”,<br />

Arte Lombarda, N.S. 117, 2, 1996, pp. 123-<br />

124<br />

[3] Codex Vallardi, accession number 2376,<br />

Louvre Museum<br />

Miklós Szentkirályi is a conservator-restorer of<br />

paintings and Head of <strong>the</strong> Department of Restoration<br />

at <strong>the</strong> Szépművészeti Múzeum (Museum of<br />

Fine Arts), Budapest. He initiated his training in<br />

1968-1973 in Painting studies at <strong>the</strong> Academy<br />

of Fine Arts “Ion Andreescu” in Cluj-Napoca, Romania,<br />

at <strong>the</strong> Master class of prof. Gábor Miklóssy,<br />

painter artist, and in 1974-1977 he performed an<br />

M.A. in Conservation Arts, specializing in paintings,<br />

at <strong>the</strong> Department of Conservation Training<br />

at <strong>the</strong> Hungarian Academy of Fine Arts, Budapest,<br />

in <strong>the</strong> master class of professor Dezső Varga. In<br />

2006 he obtained Dr. Habil. (D.Sc. Equivalent)<br />

from <strong>the</strong> Hungarian Art University. He is also a<br />

member of <strong>the</strong> Hungarian Art Academy since<br />

2010.<br />

e-<strong>conservation</strong><br />

59


"THE ANNUNCIATION"<br />

BY COLA PETRUCCIOLI (1380)<br />

The Restoration of <strong>the</strong> Transferred Wall<br />

Painting<br />

by Ildikó Jeszeniczky<br />

Restoration done by Ildikó Jeszeniczky and Kornélia Forrai<br />

Article translated by Barbara and Stevin John Davidson and originally published<br />

in <strong>the</strong> Proceedings of <strong>the</strong> 8 th International Seminar on Restoration, that took<br />

place in September 24-26, 2008 in Handlová, The Slovak Republic, organized<br />

by <strong>the</strong> Chamber of Restorers.


"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

Introduction<br />

In <strong>the</strong> 90ies of <strong>the</strong> 19 th century, Károly Pulszky,<br />

<strong>the</strong> <strong>the</strong>n director of <strong>the</strong> State Gallery in Budapest,<br />

enriched <strong>the</strong> collection of <strong>the</strong> Gallery with many<br />

art objects, panel paintings and frescoes, which<br />

he bought during his travels in Italy from palaces<br />

and churches condemned for demolition or assigned<br />

for reconstruction.<br />

Artworks got into his hands mainly through antiquity<br />

dealers, so not always he managed to find<br />

out <strong>the</strong>ir origin. Sometimes, such as in <strong>the</strong> case of<br />

<strong>the</strong> Annunciation wall painting, he discovered <strong>the</strong>m<br />

in situ and ordered <strong>the</strong>ir removal directly from <strong>the</strong><br />

original building and <strong>the</strong>ir following restoration.<br />

In September 1894, through <strong>the</strong> antiquarian<br />

Marian Rocchi, he purchased <strong>the</strong> Annunciation<br />

fresco, located on a side wall, toge<strong>the</strong>r with <strong>the</strong><br />

frescoes of allegoric women’s figures originally<br />

painted on <strong>the</strong> ceiling of <strong>the</strong> first floor of Palazzo<br />

Isidori in Perugia.<br />

The wall painting transferred onto canvas is now<br />

in Budapest, kept as an important example of<br />

<strong>the</strong> late Gothic Umbrian painting. According to<br />

<strong>the</strong> catalogue of <strong>the</strong> Szépművészeti Museum, <strong>the</strong><br />

artwork was created around <strong>the</strong> year 1380 by <strong>the</strong><br />

artist Cola Petruccioli for <strong>the</strong> wall of <strong>the</strong> first floor<br />

of <strong>the</strong> palace, originally used as a chapel.<br />

The scene is depicted in a Gothic interior, on <strong>the</strong><br />

left side a kneeling angel brings <strong>the</strong> message to<br />

Mary, who is represented on <strong>the</strong> right side of <strong>the</strong><br />

painting sitting in front of a lecture dais. In <strong>the</strong><br />

missing part it was probably painted <strong>the</strong> dove of<br />

<strong>the</strong> Holy Ghost. The painting was executed in fresco<br />

technique and is decorated around <strong>the</strong> edges with<br />

repeated motifs. The plaster haloes were covered<br />

with a coloured metal leaf which could be used<br />

as an imitation of gold.<br />

Palazzo Isidori, Perugia.<br />

In <strong>the</strong> past decade art historians succeed to locate<br />

<strong>the</strong> Palazzo Isidori in Perugia, where <strong>the</strong> restoration<br />

of <strong>the</strong> remaining frescoes from <strong>the</strong> series of<br />

wall paintings is now undergoing.<br />

About <strong>the</strong> sale and transfer of <strong>the</strong> wall paintings a<br />

few written documents were preserved, <strong>the</strong> oldest<br />

from <strong>the</strong> year 1871 in which <strong>the</strong> owner Francesco<br />

Bassardini reports in a letter to <strong>the</strong> mayor<br />

that he intends to remove some of <strong>the</strong> frescoes<br />

from <strong>the</strong> first floor of <strong>the</strong> palace and sell <strong>the</strong>m to<br />

<strong>the</strong> city. As <strong>the</strong> mayor did not respond to Bassardini’s<br />

letter <strong>the</strong> inheritors repeated <strong>the</strong> offer a<br />

few years later. In May 1889, <strong>the</strong> government of<br />

<strong>the</strong> city Perugia named a delegation with three<br />

specialist members to judge <strong>the</strong> state and importance<br />

of <strong>the</strong> frescoes. The report of <strong>the</strong> specialists<br />

and <strong>the</strong> request of <strong>the</strong> owners was not enough to<br />

persuade <strong>the</strong> mayor to buy <strong>the</strong> frescoes. Five years<br />

later, Károly Pulszky appreciated <strong>the</strong>ir artistic<br />

value, ordered <strong>the</strong>ir detachment and paid <strong>the</strong>ir<br />

purchase price.<br />

e-<strong>conservation</strong><br />

61


BY ILDIKÓ JESZENICZKY<br />

Conservation-restoration<br />

In <strong>the</strong> summer of 2005, toge<strong>the</strong>r with <strong>the</strong> colleague<br />

Kornélia Forray, <strong>the</strong> present author was entrusted<br />

<strong>the</strong> restoration of this wall painting by <strong>the</strong> museum.<br />

The restoration works were preceded by a<br />

series of detailed analysis and investigations. The<br />

research comprised <strong>the</strong> identification and ga<strong>the</strong>ring<br />

of all possible documents, art historical researches<br />

and archival photographs, and <strong>the</strong> collection<br />

of <strong>the</strong> restoration documentation of <strong>the</strong><br />

frescoes from this cycle, such as procedures reports<br />

and specialised articles. In <strong>the</strong> summer of<br />

2005 we travelled to Perugia to study in situ <strong>the</strong><br />

fragments of frescoes from Palazzo Isidori belonging<br />

to <strong>the</strong> same cycle of wall paintings as The Annunciation,<br />

which were uncovered in 1994.<br />

We were guided through <strong>the</strong> palace by Ms. Paola<br />

Passalaqua, responsible of <strong>the</strong> frescoes <strong>conservation</strong>.<br />

The palace is owned by <strong>the</strong> University of<br />

Perugia and at <strong>the</strong> time of our visit it was under<br />

renovation. The research performed on site was<br />

helpful in drawing up <strong>the</strong> restoration proposal<br />

and also influenced <strong>the</strong> proceeding of <strong>the</strong> individual<br />

stages of restoration itself. An important<br />

aspect was <strong>the</strong> surveying of <strong>the</strong> uneven surface<br />

of <strong>the</strong> preserved wall paintings fragments. We<br />

could see that <strong>the</strong> surface is not smooth, but also<br />

not as wavy as of <strong>the</strong> Annunciation, and that <strong>the</strong>y<br />

have quite different characters. We came to <strong>the</strong><br />

conclusion that <strong>the</strong> surface of <strong>the</strong> in situ fresco<br />

fragments is wavy due to <strong>the</strong> influence of <strong>the</strong><br />

masonry and <strong>the</strong> plastering method, while <strong>the</strong><br />

waving of <strong>the</strong> transferred painting was created<br />

unambiguously by <strong>the</strong> creasing of <strong>the</strong> canvas.<br />

Ms. Paola Passalaqua explained <strong>the</strong> difficulties<br />

met during <strong>the</strong> reattachment and <strong>conservation</strong><br />

of <strong>the</strong> wall paintings, such as <strong>the</strong> detachment of<br />

individual layers that lost adherence amongst<br />

<strong>the</strong>mselves and to <strong>the</strong> wall, and <strong>the</strong> weakened<br />

The Annunciation, photography in grazing light.<br />

62 e-<strong>conservation</strong>


"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

binding of <strong>the</strong> plaster. These problems were similar<br />

to those experiences by us with <strong>the</strong> thin intonaco<br />

that was removed toge<strong>the</strong>r with <strong>the</strong> paint layer,<br />

which was also very brittle.<br />

During our visit, we also surveyed <strong>the</strong> net system<br />

used for attachment of <strong>the</strong> plaster on <strong>the</strong><br />

ceiling and <strong>the</strong> ways of making and laying <strong>the</strong><br />

beams.<br />

Based on <strong>the</strong> stylistic and technical analysis of<br />

<strong>the</strong> Annunciation fresco we concluded that it was<br />

undoubtedly created in <strong>the</strong> same period as <strong>the</strong><br />

preserved fragments, with which it is related in a<br />

number of morphological details such as, for example,<br />

<strong>the</strong> decorative frame with a bordure motif.<br />

If we compare <strong>the</strong> fragments preserved in situ and<br />

<strong>the</strong> allegoric female figures from <strong>the</strong> ceiling with<br />

<strong>the</strong> depiction of <strong>the</strong> Annunciation, it is obvious<br />

that <strong>the</strong> latter can be considered <strong>the</strong> most important<br />

piece of <strong>the</strong> series because of its location within<br />

<strong>the</strong> fresco ensemble. Written documents mention<br />

that by entering <strong>the</strong> Palazzo, <strong>the</strong> visitor first<br />

laid eyes on this centrally positioned painting.<br />

The painting was probably seriously damaged by<br />

<strong>the</strong> transfer. The choice of <strong>the</strong> finely woven canvas<br />

onto which <strong>the</strong> fresco was transferred was not <strong>the</strong><br />

best one due to <strong>the</strong> bad properties of <strong>the</strong> canvas.<br />

It was probably due to this reason that <strong>the</strong> painting<br />

of <strong>the</strong> allegoric female figures from <strong>the</strong> ceiling<br />

was embedded in plaster on copper net after<br />

having been transferred. The size of <strong>the</strong> painting<br />

today is <strong>16</strong>2 x 238 cm. It was glued onto a roughly<br />

woven sackcloth and it was stretched onto a frame<br />

reinforced on <strong>the</strong> middle, with <strong>the</strong> possibility of<br />

additional stretching by <strong>the</strong> insertion of corner<br />

wedges. The stretcher was damaged in several<br />

places. The back side was coated with a thick layer<br />

Right: Details of Mary's hair and angel's portrait.<br />

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BY ILDIKÓ JESZENICZKY<br />

UV luminescence of <strong>the</strong> Annunciation.<br />

of lithopone mixed with bone glue. This was done<br />

most likely to stabilise <strong>the</strong> fabric.<br />

The stretcher was crimped and hardened on its<br />

entire surface, with many depressions and uneven<br />

areas. The layer of <strong>the</strong> plaster was strongly<br />

fissured and <strong>the</strong> material compactness was weak.<br />

On big areas (e.g. on Mary’s cloths, on <strong>the</strong> area<br />

of a stain as big as a few palms, between two figures<br />

about a half square meter, along <strong>the</strong> cracks,<br />

etc.) <strong>the</strong> original plaster and <strong>the</strong> colour layer were<br />

completely missing. A prolonged joint is visible<br />

in <strong>the</strong> middle of <strong>the</strong> painting, on <strong>the</strong> side of <strong>the</strong><br />

angel, proving that <strong>the</strong> fresco was removed in two<br />

parts and was connected again after detachment.<br />

In this area, <strong>the</strong> tones of <strong>the</strong> retouches applied<br />

during various interventions altered with time<br />

and <strong>the</strong> entire surface was dirty.<br />

IR reflectography of <strong>the</strong> portraits.<br />

The documentation comprising non-destructive<br />

analysis of <strong>the</strong> painting (by grazing light, UV luminescence<br />

and IR photography) and <strong>the</strong> results<br />

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"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

of <strong>the</strong> laboratory analysis were <strong>the</strong> basis for defining<br />

<strong>the</strong> intervention methodology, <strong>the</strong> choice<br />

of materials used and technologies.<br />

The UV luminescence showed <strong>the</strong> existence of<br />

various restoration interventions, <strong>the</strong> presence<br />

of dirt and <strong>the</strong> extent of degradation of <strong>the</strong> <strong>conservation</strong><br />

materials which were visible in different<br />

colour tones. According to historical documents,<br />

traces of 4 to 5 interventions could be identified.<br />

IR reflectography of some details of <strong>the</strong> Annunciation.<br />

IR photography revealed <strong>the</strong> underdrawing and<br />

<strong>the</strong> various pigments that appeared in different<br />

characteristic colours and depths. The cross-sections<br />

of pigment and powder samples gave information<br />

about <strong>the</strong> visible layers of colours and plaster,<br />

<strong>the</strong> particle size of <strong>the</strong> pigments and <strong>the</strong>ir<br />

optical properties.<br />

It was assessed that <strong>the</strong> wall painting was detached<br />

with <strong>the</strong> plaster and that <strong>the</strong> original pigments<br />

were:<br />

- Cinnabar, found on Mary’s clo<strong>the</strong>s. This natural,<br />

mineral pigment was, according to Andrea Pozzo,<br />

“a very popular colour, but unstable with lime. If<br />

<strong>the</strong> painting is under a roof, it is likely to be used,<br />

but it has to be adjusted for wall painting in this<br />

way: put <strong>the</strong> pigment dust into a ceramic container<br />

and pour over water which you use for slaking of<br />

<strong>the</strong> lime; strain it off and again add lime water<br />

and repeat this a few times. In this way <strong>the</strong> cinnabar<br />

connects with <strong>the</strong> properties of <strong>the</strong> lime<br />

and will never lose <strong>the</strong>m”.<br />

- Natural lapis lazuli, found on Mary’s cloak and<br />

on <strong>the</strong> ribbon of <strong>the</strong> angel’s clo<strong>the</strong>s. This pigment<br />

was spread in Europe mainly in medieval times,<br />

although it can sporadically be found also in<br />

baroque paintings. The use of this pigment suggests<br />

a rich sponsor as it was used only in small<br />

amounts and only in quality artworks.<br />

- Ferric red, on <strong>the</strong> angel’s cloak. This natural earthy<br />

pigment, ferric oxide, is named according to <strong>the</strong><br />

locality where it is found. The colour changes according<br />

to <strong>the</strong> content of hydrides and anhydrides.<br />

Pozzo describes it as “red ochre (Terra rossa), like<br />

o<strong>the</strong>r earthy colours, is great for fresco. It is used<br />

for flesh, drapery and also for o<strong>the</strong>rs”.<br />

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BY ILDIKÓ JESZENICZKY<br />

- Natural sienna, used for Mary’s hair. It is a special<br />

ochre, which is named after a well-known Tuscany<br />

city. By microscopic and chemical analysis<br />

it is ordered into <strong>the</strong> same group of pigments as<br />

ferric oxide. By Pozzo, “it is used for shading of<br />

yellow draperies.”<br />

- Yellow ochre, found on Mary’s lecture dais. It is<br />

a hydrate of ferric oxide with various composition.<br />

Pozzo defines it as “light yellow ochre is <strong>the</strong> pigment<br />

with light yellow and dark yellow colour,<br />

which is found in <strong>the</strong> surroundings of Rome”.<br />

The presence of ochre was also confirmed with UV<br />

due to its typical colour luminescence . Analysis<br />

of its additives (soil, silicates, etc.) explains <strong>the</strong><br />

creation of <strong>the</strong> blisters and <strong>the</strong> detachment of <strong>the</strong><br />

layer of ochre.<br />

- Green earth, used at <strong>the</strong> background behind<br />

<strong>the</strong> reading dais. A typical earthy pigment, it is<br />

mentioned by Pozzo as “in fresco painting <strong>the</strong><br />

only green colour for painting draperies is from<br />

Verona, because all o<strong>the</strong>r artificially made colours<br />

do not tolerate lime”. We suppose that it<br />

was also used for obtaining <strong>the</strong> flesh tones.<br />

Detail of <strong>the</strong> back of <strong>the</strong> painting in grazing light.<br />

- White. Highlights were obviously made with<br />

lime, calcium carbonate. Different variations are<br />

known: chalk, lime, shell, egg shell, corals, etc.<br />

Consolidation with Plextol B500 of Mary's plaster halo.<br />

- Carbon black, pigment found in <strong>the</strong> layers of<br />

under painting and mixed in some colours, as<br />

wooden coal.<br />

After securing and injecting <strong>the</strong> detached layers<br />

of <strong>the</strong> plaster and colour, it was proceeded to <strong>the</strong><br />

removal of <strong>the</strong> painting from <strong>the</strong> old stretcher<br />

frame. The detached creases of <strong>the</strong> canvas were<br />

impregnated with BEVA 371 which was also used<br />

to reinforce and stabilize <strong>the</strong> edges, by ironing<br />

strips of linen canvas onto <strong>the</strong> original canvas<br />

support.<br />

Thus, <strong>the</strong> painting was stretched onto a new, temporary<br />

support made-to-measure so that in its<br />

stretched state we could eliminate <strong>the</strong> characteristics<br />

that were improper to a fresco painting,<br />

mainly <strong>the</strong> unevenness of <strong>the</strong> surface, without<br />

<strong>the</strong> possible creasing of <strong>the</strong> canvas. While on horizontal<br />

position <strong>the</strong> painting was steamed and<br />

softened after a gradual stretching using <strong>the</strong><br />

corner wedges, and it was weighted down with<br />

marble plates. This process was repeated a few<br />

times within one month.<br />

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"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

Flattening of <strong>the</strong> canvas around <strong>the</strong> edges and of <strong>the</strong> surface by <strong>the</strong> application of heavy weights.<br />

The painting was altered by various <strong>conservation</strong><br />

materials from <strong>the</strong> numerous interventions and<br />

retouched a few times. Cleaning was only possible<br />

by <strong>the</strong> application of poultices with ammonium<br />

carbonate and ammonium hydroxide. Selecton B<br />

mixed with diatomic soil 1 was applied onto <strong>the</strong><br />

painting surface on 2 – 3 dm 2 and after a certain<br />

time <strong>the</strong> dirt was washed off with water. After<br />

cleaning it was possible to assess <strong>the</strong> real state<br />

of degradation and <strong>the</strong> extent of damages in proportion<br />

with <strong>the</strong> original parts, but also <strong>the</strong> richness<br />

and <strong>the</strong> fine harmony characteristic for <strong>the</strong><br />

colour scheme of this painting.<br />

Cleaning was proceeded by <strong>the</strong> consolidation of<br />

<strong>the</strong> powdering plaster and <strong>the</strong> correction of <strong>the</strong><br />

deformed halos, which were pressed back into<br />

shape in wet state. The canvas detached from<br />

<strong>the</strong> plaster was consolidated from <strong>the</strong> back and<br />

secured on its position with Plextol B500 adhesive.<br />

The missing parts of <strong>the</strong> plaster were filled and<br />

<strong>the</strong> whole was reinforced with thin woven textile<br />

made of artificial threads.<br />

A project was developed for a new stretcher with<br />

reinforcement on <strong>the</strong> back and <strong>the</strong> possibility of<br />

stretching by inserting additional wedges. The<br />

Cleaning of <strong>the</strong> painting by <strong>the</strong> application of poultices with Selecton B and diatomic soil (left) and aspect after cleaning (right).<br />

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BY ILDIKÓ JESZENICZKY<br />

Above: Cleaning of <strong>the</strong> painting by <strong>the</strong> application of poultices with solvent.<br />

Below: Consolidation and backing of <strong>the</strong> edges with Beva 371 and stripes of new canvas. Integration of <strong>the</strong> missing areas was<br />

done by filling with mortar similar in grain and texture with <strong>the</strong> original.<br />

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"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

stretching of <strong>the</strong> painting was performed by applying<br />

strips of canvas with adhesive on <strong>the</strong> edges<br />

in order to streng<strong>the</strong>n <strong>the</strong>m, edges that were<br />

<strong>the</strong>n folded back and ironed onto <strong>the</strong> original<br />

canvas. The painting was <strong>the</strong>n mounted onto <strong>the</strong><br />

stretcher by hammering metal grommets and<br />

screws in doubled layer of canvas of <strong>the</strong> edges.<br />

The aes<strong>the</strong>tical treatment started by filling <strong>the</strong><br />

lacunas of <strong>the</strong> plaster in all those places where its<br />

stability required it. The mortar used was made of:<br />

1 part of quartzite powder, 1 part of calcite powder,<br />

1 part of kaolin, 3 parts of dolomite 2 , rabbit glue<br />

7% and a little Plextol B500.<br />

Aspect of <strong>the</strong> painting after transfer onto <strong>the</strong> new stretcher<br />

and cleaning of <strong>the</strong> surface.<br />

Where possible, <strong>the</strong> missing parts were retouched for aes<strong>the</strong>tical purposes. From left to right: before <strong>conservation</strong>, after filling<br />

<strong>the</strong> lacuna and during retouching, and final aspect after reintegration by tratteggio.<br />

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BY ILDIKÓ JESZENICZKY<br />

Detail after <strong>conservation</strong>-restoration. Angel (above) and<br />

portrait of Virgin Mary (below right).<br />

The aes<strong>the</strong>tical approach was based on consulting<br />

with specialists and on <strong>the</strong> experience accumulated<br />

during one year treatment of <strong>the</strong> painting. We got<br />

to <strong>the</strong> conclusion that due to <strong>the</strong> unsatisfactory<br />

amount of information on <strong>the</strong> morphology of <strong>the</strong><br />

original painting, <strong>the</strong> largest lacunas will not be<br />

reconstructed, <strong>the</strong>se areas being better integrated<br />

into <strong>the</strong>ir surrounding by filling with neutral plaster.<br />

Smaller lacunas which could be surely retouched<br />

according to <strong>the</strong>ir surrounding context, were reconstructed<br />

for <strong>the</strong> sake of <strong>the</strong> aes<strong>the</strong>tical integrity.<br />

The architecture and interior furnishing surrounding<br />

<strong>the</strong> figures were represented without<br />

perspective, according to <strong>the</strong> style of <strong>the</strong> époque;<br />

after sketching <strong>the</strong> system of <strong>the</strong> composition,<br />

some of its parts could be reconstructed.<br />

The grazed parts were retouched only in those<br />

cases when <strong>the</strong>ir image was disturbing <strong>the</strong> reading<br />

of <strong>the</strong> painting.<br />

Besides <strong>the</strong> preservation of <strong>the</strong> original material<br />

quality, our main goal was to re-establish of <strong>the</strong><br />

author’s original intent, returning <strong>the</strong> internal<br />

balance of <strong>the</strong> painting’s aes<strong>the</strong>tical value that<br />

mediates <strong>the</strong> metaphysical message.<br />

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"THE ANNUNCIATION" BY COLA PETRUCCIOLI<br />

Angel. Detail after <strong>conservation</strong>-restoration.<br />

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BY ILDIKÓ JESZENICZKY<br />

Virgin Mary. Detail of <strong>the</strong> painting after restoration.<br />

72 e-<strong>conservation</strong>


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No. <strong>16</strong>, October 2010<br />

LICENCE<br />

ISSN: <strong>16</strong>46-9283<br />

Registration Number<br />

125248<br />

Entidade Reguladora<br />

para a Comunicação Social<br />

Property<br />

e-<strong>conservation</strong>line, Teodora Poiata<br />

Periodicity<br />

Bimonthly<br />

Cover<br />

Detail from <strong>the</strong> detached mural painting The Annunciation<br />

by Cola Petruccioli (1380), Szépművészeti Museum, Hungary.<br />

Photo by Ildikó Jeszeniczky<br />

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Editors<br />

Teodora Poiata, Anca Nicolaescu<br />

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Daniel Cull<br />

Graphic Design and Photography<br />

Anca Poiata, Radu Matase<br />

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